{"title":"研究、开发和实施利用 X 射线荧光法测定多层和多组分涂层表面密度和元素质量分数的方法","authors":"A. S. Vasiliev","doi":"10.20915/2077-1177-2024-20-2-99-114","DOIUrl":null,"url":null,"abstract":"Metal coatings provide products with the necessary technical characteristics; in particular, they increase corrosion resistance and protect against mechanical abrasion. The application of metal coatings is a promising direction and is widely used in mechanical engineering, metallurgy, and other industries. Therefore, studying the properties and improving the technology of applying metal coatings is a significant and sought-after line of activity for metrology researchers. The needs of industry in the field of monitoring the parameters of single-layer and single-component coatings in the Russian Federation are fully satisfied. At the beginning of this study, the Federal Information Fund for Ensuring the Uniformity of Measurements provided a comprehensive list of reference materials of surface density and thickness of single-layer onecomponent coatings that were tested using the State Primary Standard for units of surface density and mass fraction of elements in coatings GET 168-2015. The needs for testing, verification, and calibration of instruments for measuring surface density, thickness, and chemical composition of multilayer and multicomponent coatings remained not fully met, which became the starting point for this research.The research presented in the article was carried out in order to develop methods for determining the surface density and mass fraction of elements for multilayer and multicomponent coatings on GET 168-2015. At the same time, the problem of developing a set of reference materials of surface density and mass fraction of elements in two-layer and two-component coatings for metrological support of the corresponding measuring instruments was solved.The article fully reveals the content of the work to improve metrological support for measuring surface density, thickness, and mass fraction of elements in coatings, taking into account the needs of industry in the field of monitoring coating parameters and the variety of measurement tasks that are constantly expanding.","PeriodicalId":324937,"journal":{"name":"Measurement Standards. 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引用次数: 0
摘要
金属涂层为产品提供了必要的技术特性,尤其是提高了耐腐蚀性和防止机械磨损。金属涂层的应用是一个前景广阔的方向,在机械工程、冶金和其他行业得到广泛应用。因此,研究金属镀层的性能和改进其应用技术是计量学研究人员的一项重要而热门的活动。在俄罗斯联邦,单层和单组分涂层参数监测领域完全可以满足工业需求。在本研究开始时,"确保测量统一性联邦信息基金 "提供了一份单层单组分涂层表面密度和厚度参考材料的综合清单,该清单使用 GET 168-2015 表层密度和涂层中元素质量分数单位的国家初级标准进行了测试。多层和多组分涂层的表面密度、厚度和化学成分测量仪器的测试、验证和校准需求仍未得到完全满足,这成为本研究的出发点。文章中介绍的研究是为了开发测定 GET 168-2015 多层和多组分涂层的表面密度和元素质量分数的方法。同时,还解决了为相应测量仪器提供计量支持而开发一套双层和双组分涂层表面密度和元素质量分数参考材料的问题。文章充分揭示了改进涂层表面密度、厚度和元素质量分数测量计量支持的工作内容,同时考虑到了工业界在涂层参数监测领域的需求以及不断扩大的测量任务种类。
Research, Development and Implementation of Methods for Determining Surface Density and Mass Fraction of Elements for Multilayer and Multicomponent Coatings by X-Ray Fluorescence Method
Metal coatings provide products with the necessary technical characteristics; in particular, they increase corrosion resistance and protect against mechanical abrasion. The application of metal coatings is a promising direction and is widely used in mechanical engineering, metallurgy, and other industries. Therefore, studying the properties and improving the technology of applying metal coatings is a significant and sought-after line of activity for metrology researchers. The needs of industry in the field of monitoring the parameters of single-layer and single-component coatings in the Russian Federation are fully satisfied. At the beginning of this study, the Federal Information Fund for Ensuring the Uniformity of Measurements provided a comprehensive list of reference materials of surface density and thickness of single-layer onecomponent coatings that were tested using the State Primary Standard for units of surface density and mass fraction of elements in coatings GET 168-2015. The needs for testing, verification, and calibration of instruments for measuring surface density, thickness, and chemical composition of multilayer and multicomponent coatings remained not fully met, which became the starting point for this research.The research presented in the article was carried out in order to develop methods for determining the surface density and mass fraction of elements for multilayer and multicomponent coatings on GET 168-2015. At the same time, the problem of developing a set of reference materials of surface density and mass fraction of elements in two-layer and two-component coatings for metrological support of the corresponding measuring instruments was solved.The article fully reveals the content of the work to improve metrological support for measuring surface density, thickness, and mass fraction of elements in coatings, taking into account the needs of industry in the field of monitoring coating parameters and the variety of measurement tasks that are constantly expanding.