纳米级零价银和氧化石墨烯纳米颗粒:简易合成与表征

Nouran Yousri, Hesham H. El-Feky, Mostafa Y. Nassar, Alaa S. Amin
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引用次数: 0

摘要

我们在此报告一种以抗坏血酸/淀粉混合物为还原剂制备零价银纳米粒子的直接而简便的水热法。制备的零价银纳米粒子的平均结晶尺寸约为 46.7 nm。利用傅立叶变换红外光谱、FE-SEM 和 XRD 分析对零价银纳米产品进行了表征。此外,这项研究还展示了一种改进的氧化石墨烯纳米粒子合成方法。所制备的氧化石墨烯纳米粒子的平均结晶尺寸约为 6.0 纳米。还利用傅立叶变换红外光谱、FE-SEM 和 XRD 分析对氧化石墨烯纳米粒子进行了表征。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Nanoscale Zero-valent Silver and Graphene Oxide Nanoparticles: Facile Synthesis and Characterization
We herein report a direct and facile hydrothermal method for the preparation of zero-valent silver nanoparticles using a mixture of ascorbic acid/starch as a reducing agent. The average crystallite size of the prepared Ag0 nanoparticles was ca. 46.7 nm. The zero-valent silver nano-products were characterized by using FT-IR, FE-SEM, and XRD analyses. In addition, this work shows an improved synthesis of graphene oxide nanoparticles. The average crystallite size of the prepared graphene-oxide nanoparticles was ca. 6.0nm. The graphene oxide nanoparticles were also characterized by using FT-IR, FE-SEM, and XRD analyses.
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