合成 pva 纳米纤维,改善 PMMA 基质在义齿基托应用中的机械和热性能

Elaf J. Mohamed, Hanaa J. Kadhim, Masar N. Obaid
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引用次数: 0

摘要

本研究尝试用聚乙烯醇电纺纳米纤维制备 PMMA 纳米复合材料样品。纳米纤维加固层有一层、两层和三层。此外,还使用了一滴(0.01 克)和三滴豆蔻油。使用差示热量计进行了热实验,包括 Tg 和热解离点的实验。对样品进行了机械测试,包括压缩测试,以确定伸长特性、压缩强度、杨氏模量、屈服强度和韧性。所有样品还进行了冲击强度测试。结果表明,由于纳米纤维的存在,Tg 点从 136 摄氏度升高到 195 摄氏度,277 摄氏度为热分解点。根据机械性能数据,冲击强度随着纳米纤维比例的增加而增加,当一滴豆蔻油与极少量(0.01 克)材料混合时,冲击强度进一步增加。此外,由于纳米纤维和一滴豆蔻油的存在,样品不容易破碎。此外,研究还表明,样品的强度增加到了 195 kJ/m2,0.02 重量百分比的纤维也达到了最大强度值。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Síntesis de nanofibras de pva para mejorar las propiedades mecánicas y térmicas de la matriz de PMMA para aplicaciones en bases de prótesis dentales
This study attempts to prepare PMMA nano-composite samples armed with polyvinyl alcohol electrospun nanofibers. One layer, two layers, and three layers of nanofiber reinforcement were all utilized. As well as, one drop (0.01 g) and three drops of the cardamom oil were used. Using a differential calorimeter, thermal experiments were carried out, including those for the Tg and the thermal dissociation point. Mechanical tests were conducted on the samples, including compression testing to determine the elongation characteristics, compressive strength, Young's modulus, yield strength, and toughness. All samples were also subjected to an impact strength test. Results showed that the Tg point increased due to the presence of nanofibers from 136 to 195 Celsius, and that 277 Celsius was the thermal breakdown point. According to the mechanical property data, the impact strength increased as the percentage of nanofibers rose and increased further when one drop of cardamom oil was mixed with a very tiny amount (0.01 g) of material. Additionally, it was noted that the samples did not break easily since nanofibers and a drop of cardamom oil were present. Additionally, it was demonstrated that the sample's strength increased to 195 kJ/m2, as well as 0.02 weight % of fibers, the maximum strength value.
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