{"title":"利用桑叶提取物在室温下生物合成单分散金纳米粒子并确定其特性","authors":"C. Dong, R. Fu, S. Yu, X. Guo, W. Chen","doi":"10.1134/S1990793124020064","DOIUrl":null,"url":null,"abstract":"<p>In this research, spherical and small size gold nanoparticles were successfully prepared by a cost-effective, eco-friendly green approach using mulberry leaf extract as both reducing and stabilizing agent. The reducing potential of mulberry leaf extract was studied for the synthesis of gold nanoparticles without adding any external reducing agents. The formation of gold nanoparticles was confirmed by the change of color. The prepared gold nanoparticles were characterized by UV-visible absorption spectroscopy, dynamic light scattering, scanning electron microscope, transmission electron microscopy, fourier transform infrared and powder X-ray diffraction. The absorbance peak which found at 560 nm in UV-vis spectroscopy demonstrated the generation of gold nanoparticles. The fourier transform infrared elucidated that the gold nanoparticles were capped with various functional groups from extracts, keeping them from agglomeration and oxidation. The X-ray diffraction results illustrated that the particles were highly crystalline in nature. The transmission electron microscopy and scanning electron microscope showed the particles were small and spherical. The effect of reaction temperature, amount of chloroauric acid solution and extracts was also investigated. The results demonstrated that these parameters play vital roles in the production of gold nanoparticles.</p>","PeriodicalId":768,"journal":{"name":"Russian Journal of Physical Chemistry B","volume":null,"pages":null},"PeriodicalIF":1.4000,"publicationDate":"2024-05-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Biosynthesis and Characterization of Monodisperse Gold Nanoparticles using Mulberry Leaf Extract at Room Temperature\",\"authors\":\"C. Dong, R. Fu, S. Yu, X. Guo, W. Chen\",\"doi\":\"10.1134/S1990793124020064\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>In this research, spherical and small size gold nanoparticles were successfully prepared by a cost-effective, eco-friendly green approach using mulberry leaf extract as both reducing and stabilizing agent. The reducing potential of mulberry leaf extract was studied for the synthesis of gold nanoparticles without adding any external reducing agents. The formation of gold nanoparticles was confirmed by the change of color. The prepared gold nanoparticles were characterized by UV-visible absorption spectroscopy, dynamic light scattering, scanning electron microscope, transmission electron microscopy, fourier transform infrared and powder X-ray diffraction. The absorbance peak which found at 560 nm in UV-vis spectroscopy demonstrated the generation of gold nanoparticles. The fourier transform infrared elucidated that the gold nanoparticles were capped with various functional groups from extracts, keeping them from agglomeration and oxidation. The X-ray diffraction results illustrated that the particles were highly crystalline in nature. The transmission electron microscopy and scanning electron microscope showed the particles were small and spherical. The effect of reaction temperature, amount of chloroauric acid solution and extracts was also investigated. The results demonstrated that these parameters play vital roles in the production of gold nanoparticles.</p>\",\"PeriodicalId\":768,\"journal\":{\"name\":\"Russian Journal of Physical Chemistry B\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":1.4000,\"publicationDate\":\"2024-05-29\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Russian Journal of Physical Chemistry B\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S1990793124020064\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"PHYSICS, ATOMIC, MOLECULAR & CHEMICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Russian Journal of Physical Chemistry B","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1134/S1990793124020064","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"PHYSICS, ATOMIC, MOLECULAR & CHEMICAL","Score":null,"Total":0}
引用次数: 0
摘要
摘要 在这项研究中,利用桑叶提取物作为还原剂和稳定剂,通过一种经济高效、生态友好的绿色方法成功制备了球形小尺寸金纳米粒子。在不添加任何外部还原剂的情况下,研究了桑叶提取物合成金纳米粒子的还原潜力。金纳米粒子的形成通过颜色的变化得到了证实。制备的金纳米粒子通过紫外-可见吸收光谱、动态光散射、扫描电子显微镜、透射电子显微镜、傅里叶变换红外和粉末 X 射线衍射进行了表征。紫外可见吸收光谱在 560 纳米处发现的吸光峰证明了金纳米粒子的生成。傅立叶变换红外光谱表明,金纳米粒子被提取物中的各种官能团封盖,使其不会聚集和氧化。X 射线衍射结果表明,金纳米颗粒具有高度结晶性。透射电子显微镜和扫描电子显微镜显示,颗粒很小,呈球形。此外,还研究了反应温度、氯磺酸溶液量和提取物的影响。结果表明,这些参数在金纳米粒子的生产中起着至关重要的作用。
Biosynthesis and Characterization of Monodisperse Gold Nanoparticles using Mulberry Leaf Extract at Room Temperature
In this research, spherical and small size gold nanoparticles were successfully prepared by a cost-effective, eco-friendly green approach using mulberry leaf extract as both reducing and stabilizing agent. The reducing potential of mulberry leaf extract was studied for the synthesis of gold nanoparticles without adding any external reducing agents. The formation of gold nanoparticles was confirmed by the change of color. The prepared gold nanoparticles were characterized by UV-visible absorption spectroscopy, dynamic light scattering, scanning electron microscope, transmission electron microscopy, fourier transform infrared and powder X-ray diffraction. The absorbance peak which found at 560 nm in UV-vis spectroscopy demonstrated the generation of gold nanoparticles. The fourier transform infrared elucidated that the gold nanoparticles were capped with various functional groups from extracts, keeping them from agglomeration and oxidation. The X-ray diffraction results illustrated that the particles were highly crystalline in nature. The transmission electron microscopy and scanning electron microscope showed the particles were small and spherical. The effect of reaction temperature, amount of chloroauric acid solution and extracts was also investigated. The results demonstrated that these parameters play vital roles in the production of gold nanoparticles.
期刊介绍:
Russian Journal of Physical Chemistry B: Focus on Physics is a journal that publishes studies in the following areas: elementary physical and chemical processes; structure of chemical compounds, reactivity, effect of external field and environment on chemical transformations; molecular dynamics and molecular organization; dynamics and kinetics of photoand radiation-induced processes; mechanism of chemical reactions in gas and condensed phases and at interfaces; chain and thermal processes of ignition, combustion and detonation in gases, two-phase and condensed systems; shock waves; new physical methods of examining chemical reactions; and biological processes in chemical physics.