香蕉皮提取物比例对可持续生态友好型氧化锌纳米粒子合成的影响

A. Alwash, Farah M. Ibrahim, Salam Mohammed
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引用次数: 0

摘要

在这项工作中,利用可持续绿色技术生产出了环保型纳米氧化锌颗粒。香蕉皮提取物被用作封端剂,其负载量分别为 5%、10%、50% 和 100%。然后在马弗炉中于 400 ºC 煅烧 3 小时。为了评估合成纳米粒子的物理和化学变化,使用了 XRD、FTIR、UV-VIS 和 SEM/EDAX。表征结果表明,所有绿色合成 ZnO NPs 样品都具有良好的结晶性和较高的相纯度。使用 Debye-Scherer 公式计算了所制备样品的平均晶粒尺寸,结果表明随着提取物用量的增加,平均晶粒尺寸在缩小。傅立叶变换红外光谱结果验证了锌盐和香蕉皮提取物之间成功的化学反应。紫外-可见光谱结果表明,在提取物添加量为 100%的情况下,晶粒尺寸定量现象会产生影响。最后,所有制备样品的扫描电镜图像都证实了样品呈球形。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Effect of Banana Peels Extract Ratio on The Sustainable Eco-Friendly Synthesis of Zinc Oxide Nanoparticles
In this work, environmentally friendly zinc oxide nanoparticles was produced using sustainable green technology. With several loading amounts, such as 5%, 10%, 50%, and 100%, the banana peel extract was utilized as a capping agent. This was followed by calcinations at 400 ºC for 3 h in a muffle furnace. To evaluate the physical and chemical change of the synthesized nanoparticles, XRD, FTIR, UV-VIS and SEM/EDAX was used. The characterization results reveald that the all the green synthesized ZnO NPs samples strongly supports the well-crystallinity with high phase purity. The average crystallite size of the prepared samples was calculated using Debye-Scherer's formula and the results shows that with an increase in extract amount, the average crystallite size was shrinking. The FTIR result verified the successful chemical reaction between zinc salt and banana peel extract. The UV-VIS results showed the effect of size quantisization phenomena at 100% extract adding. Finally, the SEM images for all the prepared samples confirm the spherical shape.
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