{"title":"使用液相色谱串联质谱法(LC MS/MS)检测大豆和小麦中的农药残留量","authors":"Jemmi Muharman, Aisyah Sabrina","doi":"10.21009/jrskt.092.02","DOIUrl":null,"url":null,"abstract":"Abstrak \nPestisida berperan penting untuk membasmi hama dan serangga dalam bidang pertanian agar diperoleh hasil pertanian yang baik. Tetapi, pestisida yang diaplikasikan pada hasil pertanian akan meninggalkan residu yang membahayakan jika dikonsumsi. Oleh sebab itu, penentian ini dilaksanakan bertujuan untuk menganalisis kadar pestisida seperti azoxystrobin, carbaryl, dan difenoconazole dalam kacang kedelai dan gandum sesuai dengan batas nilai paparan yang normal. Pengujian kadar pestisida dilakukan dengan menggunakan metode QuEChERS EN 15662:2018 menggunakan Liquid Chromatography Tandem Mass Spectrometry (LC MS/MS). Pengujian kadar residu pestisida pada kacang kedelai dan gandum memperoleh hasil yang masih memenuhi syarat PERMENTAN Nomor 53 Tahun 2018. \nKata kunci: : azoxystrobin, carbaryl, difenoconazole, gandum, kedelai, pestisida, QuEChERS \nAbstract \nPesticides play an important role in eradicating pests and insects in the agricultural sector in order to obtain good agricultural results. However, pesticides applied to agricultural products will leave residues that are dangerous if consumed. Therefore, this determination was carried out with the aim of analyzing the levels of pesticides such as azoxystrobin, carbaryl, and difenoconazole in soybeans and wheat in accordance with normal exposure value limits. Testing for pesticide levels was carried out using the QuEChERS EN 15662:2018 method using Liquid Chromatography Tandem Mass Spectrometry (LC MS/MS). 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Tetapi, pestisida yang diaplikasikan pada hasil pertanian akan meninggalkan residu yang membahayakan jika dikonsumsi. Oleh sebab itu, penentian ini dilaksanakan bertujuan untuk menganalisis kadar pestisida seperti azoxystrobin, carbaryl, dan difenoconazole dalam kacang kedelai dan gandum sesuai dengan batas nilai paparan yang normal. Pengujian kadar pestisida dilakukan dengan menggunakan metode QuEChERS EN 15662:2018 menggunakan Liquid Chromatography Tandem Mass Spectrometry (LC MS/MS). Pengujian kadar residu pestisida pada kacang kedelai dan gandum memperoleh hasil yang masih memenuhi syarat PERMENTAN Nomor 53 Tahun 2018. \\nKata kunci: : azoxystrobin, carbaryl, difenoconazole, gandum, kedelai, pestisida, QuEChERS \\nAbstract \\nPesticides play an important role in eradicating pests and insects in the agricultural sector in order to obtain good agricultural results. However, pesticides applied to agricultural products will leave residues that are dangerous if consumed. 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引用次数: 0
摘要
Abstrak Pestisida(虫害防治)是一种用于防治虫害的杀虫剂。此外,虫害也会在虫害发生时产生残留物。因此,本手册中的杀虫剂可用于防治虫害,包括唑菌酯、甲萘威和苯醚甲环唑。通过使用 QuEChERS EN 15662:2018 方法和液相色谱串联质谱法(LC MS/MS)来检测害虫。通过对杀虫剂和杀虫剂残留物的检测,可提高对 PERMENTAN Nomor 53 Tahun 2018 的认识。Kata kunci: : azoxystrobin, carbaryl, difenoconazole, gandum, kedelai, pestisida, QuEChERS Abstract Pesticides play an important role in eradication pests and insects in the agricultural sector in order to obtain good agricultural results.然而,施用在农产品上的杀虫剂会留下残留物,食用后会对人体造成危害。因此,本次测定的目的是根据正常接触值限值,分析大豆和小麦中唑氧菌酯、甲萘威和苯醚甲环唑等杀虫剂的含量。农药含量检测采用 QuEChERS EN 15662:2018 方法,使用液相色谱串联质谱法(LC MS/MS)进行。检测大豆和小麦中的农药残留量,得到的结果仍符合2018年第53号PERMENTAN的要求。关键词:唑虫酰胺、西维因、苯醚甲环唑、农药、大豆、QuEChERS、小麦
Pengujian Kandungan Residu Pestisida pada Kacang Kedelai dan Gandum menggunakan Liquid Chromatography Tandem Mass Spectrometry (LC MS/MS)
Abstrak
Pestisida berperan penting untuk membasmi hama dan serangga dalam bidang pertanian agar diperoleh hasil pertanian yang baik. Tetapi, pestisida yang diaplikasikan pada hasil pertanian akan meninggalkan residu yang membahayakan jika dikonsumsi. Oleh sebab itu, penentian ini dilaksanakan bertujuan untuk menganalisis kadar pestisida seperti azoxystrobin, carbaryl, dan difenoconazole dalam kacang kedelai dan gandum sesuai dengan batas nilai paparan yang normal. Pengujian kadar pestisida dilakukan dengan menggunakan metode QuEChERS EN 15662:2018 menggunakan Liquid Chromatography Tandem Mass Spectrometry (LC MS/MS). Pengujian kadar residu pestisida pada kacang kedelai dan gandum memperoleh hasil yang masih memenuhi syarat PERMENTAN Nomor 53 Tahun 2018.
Kata kunci: : azoxystrobin, carbaryl, difenoconazole, gandum, kedelai, pestisida, QuEChERS
Abstract
Pesticides play an important role in eradicating pests and insects in the agricultural sector in order to obtain good agricultural results. However, pesticides applied to agricultural products will leave residues that are dangerous if consumed. Therefore, this determination was carried out with the aim of analyzing the levels of pesticides such as azoxystrobin, carbaryl, and difenoconazole in soybeans and wheat in accordance with normal exposure value limits. Testing for pesticide levels was carried out using the QuEChERS EN 15662:2018 method using Liquid Chromatography Tandem Mass Spectrometry (LC MS/MS). Testing pesticide residue levels in soybeans and wheat obtained results that still met the requirements of PERMENTAN Number 53 of 2018.
Keywords: azoxystrobin, carbaryl, difenoconazole, pesticides, soybeans, QuEChERS, wheat