{"title":"用共沉淀法制备硅烷处理过的蛋壳聚氯乙烯薄膜：乙烯基三甲氧基硅烷表面处理对拉伸性能的影响","authors":"D. Kiryakova, Ganka Kolchakova","doi":"10.4028/p-gl3hot","DOIUrl":null,"url":null,"abstract":"Waste eggshell powders with a particle size of less than 0.315 μm were surface treated with vinyltrimethoxysilane. XRD, FT-IR, BET and SEM analyses were used to determine the surface characteristics of eggshells before and after silane treatment. The preparation of films of unplasticized suspension polyvinyl chloride with untreated and silane-treated eggshells was done by co-precipitation of solutions from cyclohexanone. The tensile properties of obtained films containing vinyltrimethoxysilane-treated eggshell powders were investigated and analyzed relative to the compositions with untreated powders.","PeriodicalId":507685,"journal":{"name":"Key Engineering Materials","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2024-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Preparation of Silane-Treated Eggshells Polyvinyl Chloride Films by Co-Precipitation: Effect of Vinyltrimethoxysilane Surface Treatment on the Tensile Properties\",\"authors\":\"D. Kiryakova, Ganka Kolchakova\",\"doi\":\"10.4028/p-gl3hot\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Waste eggshell powders with a particle size of less than 0.315 μm were surface treated with vinyltrimethoxysilane. XRD, FT-IR, BET and SEM analyses were used to determine the surface characteristics of eggshells before and after silane treatment. The preparation of films of unplasticized suspension polyvinyl chloride with untreated and silane-treated eggshells was done by co-precipitation of solutions from cyclohexanone. The tensile properties of obtained films containing vinyltrimethoxysilane-treated eggshell powders were investigated and analyzed relative to the compositions with untreated powders.\",\"PeriodicalId\":507685,\"journal\":{\"name\":\"Key Engineering Materials\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2024-05-14\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Key Engineering Materials\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.4028/p-gl3hot\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Key Engineering Materials","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.4028/p-gl3hot","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
用乙烯基三甲氧基硅烷对粒径小于 0.315 μm 的废弃蛋壳粉进行表面处理。利用 XRD、FT-IR、BET 和 SEM 分析确定了硅烷处理前后蛋壳的表面特性。用环己酮溶液共沉淀法制备了未经塑化的悬浮聚氯乙烯薄膜和经硅烷处理的蛋壳。研究和分析了含有乙烯基三甲氧基硅烷处理过的蛋壳粉末的薄膜的拉伸性能，并将其与未处理过的蛋壳粉末进行比较。
Preparation of Silane-Treated Eggshells Polyvinyl Chloride Films by Co-Precipitation: Effect of Vinyltrimethoxysilane Surface Treatment on the Tensile Properties
Waste eggshell powders with a particle size of less than 0.315 μm were surface treated with vinyltrimethoxysilane. XRD, FT-IR, BET and SEM analyses were used to determine the surface characteristics of eggshells before and after silane treatment. The preparation of films of unplasticized suspension polyvinyl chloride with untreated and silane-treated eggshells was done by co-precipitation of solutions from cyclohexanone. The tensile properties of obtained films containing vinyltrimethoxysilane-treated eggshell powders were investigated and analyzed relative to the compositions with untreated powders.
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