纳米颗粒改性义齿基底树脂的颜色和弯曲性能:体外比较研究

IF 2 Q2 MEDICINE, GENERAL & INTERNAL
Abdel-Naser M Emam, Karim-Eldin Ibrahim Ahmed, Adel M Shaaban, Mohammad Abdullah Alqhtani, Mohammed M Gad, Mohamed Ahmed Helal
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引用次数: 0

摘要

目的:用无机填料增强聚甲基丙烯酸甲酯(PMMA)义齿基托树脂(DBR)具有优异的性能和公认的美观性,但目前仍是一个难题。本研究旨在评估用纳米银粒子(AgNPs)和纳米二氧化锆粒子(ZNPs)改性的热聚合 DBR 材料的颜色变化、抗弯强度和弹性模量:制作了 60 个丙烯酸试样(30 个/颜色测试,30 个/挠曲性能),并根据纳米粒子的类型和添加量分为 3 组(n = 10)。第一组为未改性试样,第二组为含 0.5wt% AgNPs 的改性试样(PMMA/AgNPs),第三组为含 7.5wt% ZNPs 的改性试样(PMMA/ZNPs)。制作了圆盘形(20 × 3 毫米)和条形(65 × 10 × 2.5 毫米)试样,分别用于测量颜色和弯曲性能。分光光度计用于评估颜色变化(ΔE)。弯曲强度和弹性模量的评估采用三点弯曲试验(5 毫米/分钟)。采用 Tukey 后验法和单因素方差分析对数据进行分析,显著性水平为 P ≤ 0.05:与 PMMA/ZNPs 相比,PMMA/AgNPs 组的颜色变化明显增加。与未改性组和 PMMA/AgNPs 组相比,PMMA/ZNPs 组的抗折强度值明显最高(P < 0.001),但 PMMA/AgNPs 组与未改性组之间的抗折强度值没有显著差异(P > 0.05)。PMMA/AgNPs 对弹性模量强度的提高不显著(P = 0.09410),而 PMMA/ZNPs 则显著提高了弹性模量强度(P = 0.00396):结论:在 PMMA 中添加 AgNPs 和 ZNPs 增加了 DBR 的颜色变化,而 AgNPs 则改变了 DBR 的颜色。ZNPs 增加了 DBR 的弯曲属性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Color and flexural properties of nanoparticles-modified denture base resin: An in vitro comparative study.

Objectives: Reinforcement of polymethylmethacrylate (PMMA) denture base resins (DBRs) with inorganic fillers with superior properties and accepted aesthetics are favored and still a big dilemma. This study was undertaken to evaluate the color change, flexural strength, and modulus of elasticity of heat-polymerized DBR material modified with silver nanoparticles (AgNPs) and zirconium dioxide nanoparticles (ZNPs).

Methods: Sixty acrylic specimens (30/color test, 30/flexural properties) were fabricated and divided according to nanoparticles type and addition into 3 groups (n = 10). Group-I; unmodified specimens, Group-II; modified specimens with 0.5wt% AgNPs (PMMA/AgNPs), and Group-III; modified specimens with 7.5wt% ZNPs (PMMA/ZNPs). Disc-shape (20 × 3 mm) and bar-shape (65 × 10 × 2.5 mm) specimens were fabricated for color and flexural properties, respectively. The spectrophotometer was used for evaluation of the color change (∆E). The flexural strength and elastic modulus evaluation was carried out using a 3-point bending test (5 mm/min). Tukey's post hoc and one-way ANOVA were used to analyze the data at a significant level P ≤ 0.05.

Results: PMMA/AgNPs group exhibited a significant increase in color change when compared with PMMA/ZNPs. PMMA/ZNPs showed significantly the highest flexural strength value when compared with unmodified and PMMA/AgNPs groups (P < 0.001), however, there was an absence of significant differences in terms of flexural strength values between PMMA/AgNPs and unmodified groups (P > 0.05). PMMA/AgNPs insignificantly increased its modulus of elasticity strength (P = 0.09410) while PMMA/ZNPs significantly increased its modulus of elasticity strength (P = 0.00396).

Conclusion: The AgNPs and ZNPs addition to PMMA increased the color change and AgNPs change the color of DBRs. The flexural attributes of DBRs have been increased by ZNPs.

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来源期刊
International Journal of Health Sciences-IJHS
International Journal of Health Sciences-IJHS MEDICINE, GENERAL & INTERNAL-
自引率
15.00%
发文量
49
审稿时长
8 weeks
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