硫化镓（Ga2S3）：在无溶剂条件下合成 3,3-（芳基亚甲基）-双（4-羟基香豆素）的绿色、可重复使用且高效的纳米催化剂

IF 0.7 4区化学 Q4 CHEMISTRY, ORGANIC

Letters in Organic Chemistry Pub Date : 2024-04-30 DOI:10.2174/0115701786303227240422140153

Amol R. Parhad, Dilip S. Aute, Anil G. Gadhave, Bhagwat K. Uphade

{"title":"硫化镓（Ga2S3）：在无溶剂条件下合成 3,3-（芳基亚甲基）-双（4-羟基香豆素）的绿色、可重复使用且高效的纳米催化剂","authors":"Amol R. Parhad, Dilip S. Aute, Anil G. Gadhave, Bhagwat K. Uphade","doi":"10.2174/0115701786303227240422140153","DOIUrl":null,"url":null,"abstract":":: Our current work's primary goal is to create novel heterogeneous gallium sulfide (Ga2S3) nanocatalysts and investigate their catalytic activity in the synthesis of 3,3-(arylmethylene)-bis-(4- hydroxycoumarin) derivatives without use of solvent. FT-IR, XRD, SEM, and EDX analysis characterized the synthesized gallium sulfide (Ga2S3) nanomaterial catalysts. This method's main benefits are its short reaction time, solvent-free conditions, extremely mild reaction conditions, good product yield, and, most importantly, its ability to recover catalysts after at least four runs. background: Use nanocatalyst in multicomponent reaction. objective: To enhance the catalytic activity of nanocatalyst.","PeriodicalId":18116,"journal":{"name":"Letters in Organic Chemistry","volume":"32 1","pages":""},"PeriodicalIF":0.7000,"publicationDate":"2024-04-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Gallium Sulphide (Ga2S3): Green, Reusable, and Efficient Nanocatalyst for the Synthesis of 3,3-(arylmethylene)-bis-(4-hydroxycoumarin) Under Solvent-free Condition\",\"authors\":\"Amol R. Parhad, Dilip S. Aute, Anil G. Gadhave, Bhagwat K. Uphade\",\"doi\":\"10.2174/0115701786303227240422140153\",\"DOIUrl\":null,\"url\":null,\"abstract\":\":: Our current work's primary goal is to create novel heterogeneous gallium sulfide (Ga2S3) nanocatalysts and investigate their catalytic activity in the synthesis of 3,3-(arylmethylene)-bis-(4- hydroxycoumarin) derivatives without use of solvent. FT-IR, XRD, SEM, and EDX analysis characterized the synthesized gallium sulfide (Ga2S3) nanomaterial catalysts. This method's main benefits are its short reaction time, solvent-free conditions, extremely mild reaction conditions, good product yield, and, most importantly, its ability to recover catalysts after at least four runs. background: Use nanocatalyst in multicomponent reaction. objective: To enhance the catalytic activity of nanocatalyst.\",\"PeriodicalId\":18116,\"journal\":{\"name\":\"Letters in Organic Chemistry\",\"volume\":\"32 1\",\"pages\":\"\"},\"PeriodicalIF\":0.7000,\"publicationDate\":\"2024-04-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Letters in Organic Chemistry\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://doi.org/10.2174/0115701786303227240422140153\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, ORGANIC\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Letters in Organic Chemistry","FirstCategoryId":"92","ListUrlMain":"https://doi.org/10.2174/0115701786303227240422140153","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, ORGANIC","Score":null,"Total":0}

引用次数: 0

摘要

::我们当前工作的主要目标是创建新型异相硫化镓（Ga2S3）纳米催化剂，并研究其在不使用溶剂的情况下合成 3,3-（芳基亚甲基）-双（4-羟基香豆素）衍生物的催化活性。傅立叶变换红外光谱（FT-IR）、X射线衍射（XRD）、扫描电镜（SEM）和乙二胺四乙酸氙（EDX）分析对合成的硫化镓（Ga2S3）纳米材料催化剂进行了表征。该方法的主要优点是反应时间短、无溶剂、反应条件极其温和、产品收率高，最重要的是至少可在四次运行后回收催化剂：在多组分反应中使用纳米催化剂：提高纳米催化剂的催化活性。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

查看原文本刊更多论文

Gallium Sulphide (Ga2S3): Green, Reusable, and Efficient Nanocatalyst for the Synthesis of 3,3-(arylmethylene)-bis-(4-hydroxycoumarin) Under Solvent-free Condition

:: Our current work's primary goal is to create novel heterogeneous gallium sulfide (Ga2S3) nanocatalysts and investigate their catalytic activity in the synthesis of 3,3-(arylmethylene)-bis-(4- hydroxycoumarin) derivatives without use of solvent. FT-IR, XRD, SEM, and EDX analysis characterized the synthesized gallium sulfide (Ga2S3) nanomaterial catalysts. This method's main benefits are its short reaction time, solvent-free conditions, extremely mild reaction conditions, good product yield, and, most importantly, its ability to recover catalysts after at least four runs. background: Use nanocatalyst in multicomponent reaction. objective: To enhance the catalytic activity of nanocatalyst.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

Letters in Organic Chemistry 化学-有机化学

CiteScore

1.30

自引率

12.50%

发文量

135

审稿时长

7 months

期刊介绍： Aims & Scope Letters in Organic Chemistry publishes original letters (short articles), research articles, mini-reviews and thematic issues based on mini-reviews and short articles, in all areas of organic chemistry including synthesis, bioorganic, medicinal, natural products, organometallic, supramolecular, molecular recognition and physical organic chemistry. The emphasis is to publish quality papers rapidly by taking full advantage of latest technology for both submission and review of the manuscripts. The journal is an essential reading for all organic chemists belonging to both academia and industry.