P. Kashid, S. Mathad, Mahadev R. Shedam, Rakesh R. Shedam
{"title":"钴纳米铁氧体结构特性的镉替代物的低温化学合成与研究","authors":"P. Kashid, S. Mathad, Mahadev R. Shedam, Rakesh R. Shedam","doi":"10.4028/p-sv7exq","DOIUrl":null,"url":null,"abstract":"This article presents, the systematic and successful preparation of cadmium substituted cobalt ferrite (Co1-xCdxFe2O4) nanoparticles via simple co-precipitation method. X-ray diffraction study confirmed the prepared ferrite nanoparticles were crystallized with a mono phase cubic spinel structure of Fd3m space group. The average crystallite size (Dxrd) was increased with Cd doping content, due to the replacement of Co2+ ions by Cd2+ ions. XRD pattern revealed the high intense peak corresponds to (311) lattice plane and confirmed the formation of cubic structure ferrite nanoparticles. Morphological study was done by using SEM images. The grain size found to be increased with Cd concentration and it reaches the highest of around 0.9μm for Co0.52Cd0.48Fe2O4 composition. Fourier Transform Infrared spectroscopy of prepared samples was recorded in the range of 1000-350 cm-1, confirmed the spinel structure.","PeriodicalId":177608,"journal":{"name":"Journal of Metastable and Nanocrystalline Materials","volume":"49 3","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2024-04-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Low Temperature Chemical Synthesis and Investigation of Cadmium Substituted of Structural Properties of Cobalt Nano Ferrites\",\"authors\":\"P. Kashid, S. Mathad, Mahadev R. Shedam, Rakesh R. Shedam\",\"doi\":\"10.4028/p-sv7exq\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"This article presents, the systematic and successful preparation of cadmium substituted cobalt ferrite (Co1-xCdxFe2O4) nanoparticles via simple co-precipitation method. X-ray diffraction study confirmed the prepared ferrite nanoparticles were crystallized with a mono phase cubic spinel structure of Fd3m space group. The average crystallite size (Dxrd) was increased with Cd doping content, due to the replacement of Co2+ ions by Cd2+ ions. XRD pattern revealed the high intense peak corresponds to (311) lattice plane and confirmed the formation of cubic structure ferrite nanoparticles. Morphological study was done by using SEM images. The grain size found to be increased with Cd concentration and it reaches the highest of around 0.9μm for Co0.52Cd0.48Fe2O4 composition. Fourier Transform Infrared spectroscopy of prepared samples was recorded in the range of 1000-350 cm-1, confirmed the spinel structure.\",\"PeriodicalId\":177608,\"journal\":{\"name\":\"Journal of Metastable and Nanocrystalline Materials\",\"volume\":\"49 3\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2024-04-03\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Metastable and Nanocrystalline Materials\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.4028/p-sv7exq\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Metastable and Nanocrystalline Materials","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.4028/p-sv7exq","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Low Temperature Chemical Synthesis and Investigation of Cadmium Substituted of Structural Properties of Cobalt Nano Ferrites
This article presents, the systematic and successful preparation of cadmium substituted cobalt ferrite (Co1-xCdxFe2O4) nanoparticles via simple co-precipitation method. X-ray diffraction study confirmed the prepared ferrite nanoparticles were crystallized with a mono phase cubic spinel structure of Fd3m space group. The average crystallite size (Dxrd) was increased with Cd doping content, due to the replacement of Co2+ ions by Cd2+ ions. XRD pattern revealed the high intense peak corresponds to (311) lattice plane and confirmed the formation of cubic structure ferrite nanoparticles. Morphological study was done by using SEM images. The grain size found to be increased with Cd concentration and it reaches the highest of around 0.9μm for Co0.52Cd0.48Fe2O4 composition. Fourier Transform Infrared spectroscopy of prepared samples was recorded in the range of 1000-350 cm-1, confirmed the spinel structure.
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