{"title":"开发导电材料及其表征的可持续和高能效方法","authors":"Khalid Bashir, Dheeraj Gupta, Vivek Jain","doi":"10.1177/14644207241244600","DOIUrl":null,"url":null,"abstract":"In this study, composite castings of electrically conductive materials were prepared using electromagnetic energy of frequency 2.45 GHz. Three separate sets of castings were produced inside the domestic microwave applicator cavity, with reinforced compositions of up to 15% in steps of 5% for each composite cast (copper (Cu) + 5% molybdenum (Mo), Cu + 10% Mo, and Cu + 15% Mo). A microwave radiation exposure time of 12 min was required for the complete melting of pure copper powder. However, the addition of Mo reinforcement caused a reduction in exposure time to 11.33 min (min) for the Cu-15% Mo composite cast. The formation of different phases was revealed by the X-ray diffraction analysis of the cast samples. Only a 0.92% copper oxide phase was detected in the pure copper cast samples. The composite cast samples exhibited peaks corresponding to Cu<jats:sub>64</jats:sub>O, Cu<jats:sub>6</jats:sub>Mo<jats:sub>5</jats:sub>O<jats:sub>18</jats:sub>, and MoO<jats:sub>2</jats:sub>. Microstructure analysis demonstrated that the grains grew in an equiaxed manner with a uniform dispersion of the reinforcements. The maximum microhardness achieved is 99.2 ± 4.99 Hv for Cu + 15% Mo which is 1.66 times better than microwave-cast copper sample.","PeriodicalId":20630,"journal":{"name":"Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications","volume":"58 1","pages":""},"PeriodicalIF":2.5000,"publicationDate":"2024-04-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"A sustainable and energy efficient approach for development of electrically conductive materials and their characterizations\",\"authors\":\"Khalid Bashir, Dheeraj Gupta, Vivek Jain\",\"doi\":\"10.1177/14644207241244600\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this study, composite castings of electrically conductive materials were prepared using electromagnetic energy of frequency 2.45 GHz. Three separate sets of castings were produced inside the domestic microwave applicator cavity, with reinforced compositions of up to 15% in steps of 5% for each composite cast (copper (Cu) + 5% molybdenum (Mo), Cu + 10% Mo, and Cu + 15% Mo). A microwave radiation exposure time of 12 min was required for the complete melting of pure copper powder. However, the addition of Mo reinforcement caused a reduction in exposure time to 11.33 min (min) for the Cu-15% Mo composite cast. The formation of different phases was revealed by the X-ray diffraction analysis of the cast samples. Only a 0.92% copper oxide phase was detected in the pure copper cast samples. The composite cast samples exhibited peaks corresponding to Cu<jats:sub>64</jats:sub>O, Cu<jats:sub>6</jats:sub>Mo<jats:sub>5</jats:sub>O<jats:sub>18</jats:sub>, and MoO<jats:sub>2</jats:sub>. Microstructure analysis demonstrated that the grains grew in an equiaxed manner with a uniform dispersion of the reinforcements. The maximum microhardness achieved is 99.2 ± 4.99 Hv for Cu + 15% Mo which is 1.66 times better than microwave-cast copper sample.\",\"PeriodicalId\":20630,\"journal\":{\"name\":\"Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications\",\"volume\":\"58 1\",\"pages\":\"\"},\"PeriodicalIF\":2.5000,\"publicationDate\":\"2024-04-02\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1177/14644207241244600\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1177/14644207241244600","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
摘要
本研究利用频率为 2.45 GHz 的电磁能制备了导电材料复合铸件。在家用微波炉的炉腔内分别制备了三组铸件,每组铸件的强化成分最高为 15%,以 5%为单位(铜 (Cu) + 5%钼 (Mo)、铜 + 10%钼和铜 + 15%钼)。纯铜粉完全熔化需要 12 分钟的微波辐射时间。然而,添加 Mo 增强剂后,Cu-15% Mo 复合铸件的辐射时间缩短至 11.33 分钟。铸件样品的 X 射线衍射分析显示了不同相的形成。在纯铜铸件样品中只检测到 0.92% 的氧化铜相。复合铸件样品显示出对应于 Cu64O、Cu6Mo5O18 和 MoO2 的峰值。显微结构分析表明,晶粒以等轴的方式生长,增强体均匀分布。Cu + 15% Mo 的最大显微硬度为 99.2 ± 4.99 Hv,是微波铸造铜样品的 1.66 倍。
A sustainable and energy efficient approach for development of electrically conductive materials and their characterizations
In this study, composite castings of electrically conductive materials were prepared using electromagnetic energy of frequency 2.45 GHz. Three separate sets of castings were produced inside the domestic microwave applicator cavity, with reinforced compositions of up to 15% in steps of 5% for each composite cast (copper (Cu) + 5% molybdenum (Mo), Cu + 10% Mo, and Cu + 15% Mo). A microwave radiation exposure time of 12 min was required for the complete melting of pure copper powder. However, the addition of Mo reinforcement caused a reduction in exposure time to 11.33 min (min) for the Cu-15% Mo composite cast. The formation of different phases was revealed by the X-ray diffraction analysis of the cast samples. Only a 0.92% copper oxide phase was detected in the pure copper cast samples. The composite cast samples exhibited peaks corresponding to Cu64O, Cu6Mo5O18, and MoO2. Microstructure analysis demonstrated that the grains grew in an equiaxed manner with a uniform dispersion of the reinforcements. The maximum microhardness achieved is 99.2 ± 4.99 Hv for Cu + 15% Mo which is 1.66 times better than microwave-cast copper sample.
期刊介绍:
The Journal of Materials: Design and Applications covers the usage and design of materials for application in an engineering context. The materials covered include metals, ceramics, and composites, as well as engineering polymers.
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