MnFe2O4 纳米粒子作为一种新型磁分离纳米催化剂,用于无溶剂合成二氢吡喃 [2,3-c] 吡唑衍生物

Santosh B. Gaikwad, Kishore Puri
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引用次数: 0

摘要

本研究的重点是利用溶胶-凝胶法合成 MnFe2O4(锰铁氧体)纳米粒子。然后,我们将这些纳米颗粒用作催化剂,在特定温度下合成二氢吡喃并[2,3-c]吡唑衍生物。这种工艺的最大优点是只需很短的反应时间,而且不需要溶剂。此外,还可以通过简单的重结晶工艺提纯粗吡喃并唑衍生物。该催化剂可重复使用,可通过磁力分离,即使使用五次后仍能保持其活性。催化剂的化学完整性已通过傅立叶变换红外光谱、1H NMR 和 13C NMR 技术得到证实。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
MnFe2O4 nanoparticle as a new and magnetically separable nanocatalyst for solvent-free synthesis of dihydropyrano [2,3-c]pyrazole derivatives
This study focused on synthesising MnFe2O4 (Manganese Ferrite) nanoparticles using the sol-gel method. We then applied these nanoparticles as a catalyst for synthesising dihydropyrano[2,3-c]pyrazole derivatives at a specific temperature. The significant advantage of this process is that it requires only short reaction times and no solvents. Additionally, the crude pyranopyrazole derivatives can be purified through a simple recrystallization process. The catalyst is reusable, magnetically separable and maintains its activity even after five uses. The chemical integrity of the catalyst was confirmed through FT-IR, 1H NMR, and 13C NMR techniques.
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