采用田口方法优化 SUS 304 上二氧化钛/氧化锌混合涂层的腐蚀行为

Vandana N Mahajan, M. J. Sable, S. P. Shekhawat, Suhas R Patil
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摘要

目标确定涂覆在 SUS 上的二氧化钛/氧化锌混合物的最佳组合,以获得最小的腐蚀率。方法: 在 SUS 30 上涂覆不同的 TiO2 /ZnO 薄膜混合物:在 SUS 304 基材上涂覆不同的 TiO2 /ZnO 薄膜混合物。涂层应用采用溶胶-凝胶浸涂工艺。此外,抽出率、煅烧温度和掺杂百分比也是用于研究防腐蚀性能的参数。实验设计采用田口方法的 L9 阵列。防腐试验采用 P.G-Lyte 1.0 模型。采用电位极化法进行防腐测试。结果结果表明,氧化锌掺杂比例(60%、40% 和 20%)是控制 1 号板样品腐蚀的最重要因素。抽取速率(0.5 毫米/秒、1 毫米/秒和 1.5 毫米/秒)对涂层样品的腐蚀速率影响很小。煅烧温度(300◦C、400◦C 和 500◦C)比抽出率的影响更大。预测的腐蚀电流与实际的腐蚀电流之间有很好的一致性。新颖性:通过应用 TiO2 和 ZnO 混合物涂层来提高耐腐蚀性等机械性能,这对于提高汽车部件的耐用性至关重要。在这项研究中,通过使用不同的二氧化钛和氧化锌混合物,努力降低腐蚀率。此外,在此过程中还改变了抽出率和煅烧温度,这也是以前的研究中没有考虑到的。关键词田口方法;腐蚀电流;信噪比;涂层;实验设计
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Optimization of Corrosion Behaviour of Blended TiO2 /ZnO Coating on SUS 304 using Taguchi Method
Objectives: To determine the best combination of blends of TiO2 /ZnO coated on SUS for obtaining a minimum corrosion rate. Methods: Different TiO2 /ZnO thin film blends are coated on SUS 304 substrates. The sol-gel dip-coating process is used for coating application. Also, withdrawal rates, calcination temperature, and doping percentage are the parameters used for the study of the anti-corrosion property. L9 array, using the Taguchi method, is applied for the design of the experiment. P.G-Lyte 1.0 model was used for the anticorrosion test. The Potentiosatic polarization method was applied for anti-corrosion testing. Findings: The results show that the percentage of ZnO doping (60%, 40%, and 20%) is the most significant factor in controlling the corrosion of the sample with plate number 1. The withdrawal rate (0.5 mm/sec, 1 mm/sec, and 1.5 mm/sec) has a minimal impact on the corrosion rate of the coated sample. The calcination temperature (300◦C, 400◦C, and 500◦C) has a greater impact than the withdrawal rate. There is a good agreement between the predicted and actual corrosion current. Novelty: Investigation of mechanical properties like corrosion resistance is essential for increasing the durability of automobile components by applying a coating of blends of TiO2 and ZnO with a rare blending combination that was not applied before for the investigation. In this research, efforts are made to reduce the corrosion rate by applying different blends of TiO2 and ZnO. Also, withdrawal rate and calcination temperature are varied in the process which was also not considered in the earlier studies. Keywords: Taguchi method; Corrosion current; Signal to Noise ratio; Coating; Design of experiments
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