Chadron M. Friesen, Nathan J. Weeks, Scott T. Iacono
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引用次数: 0
摘要
利用全氟吡啶（PFP）对 1,8-二氮杂双环[5.4.0]十一-7-烯（DBU）的亲核芳香取代作用，合成了标题化合物，产量接近定量。该化合物的纯度和结构是通过核磁共振（1H、13C、19F）、气相色谱-质谱和单晶 X 射线晶体学测定的。
The title compound was synthesized at a near-quantitative yield using the nucleophilic aromatic substitution of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) with perfluoropyridine (PFP). The purity and structure were determined by NMR (1H, 13C, 19F), GC-EIMS, and single-crystal X-ray crystallography.
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