从萨尔瓦多柿叶提取物中绿色合成氧化锌纳米颗粒:表征和吸附去除甲基橙的研究

Amal S. Al Rahbi, Ahlam H. Al Mawali, Shahad S. Al Rawahi, Rima K. Al Dighishi, Fatma A. Al Abri, Anwar Ahmed, Sadik Rahman
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引用次数: 0

摘要

本研究以萨尔瓦多柿叶提取物的水溶液为封端剂,成功地绿色合成了氧化锌纳米粒子(ZnO NPs)。通过甲基橙(MO)染料去除研究了解了合成的氧化锌纳米粒子在环境中的应用。通过扫描电子显微镜(SEM)、能量色散光谱、傅立叶变换红外光谱(FTIR)、X 射线衍射(XRD)和紫外可见光谱(UV-Vis)对合成氮氧化物的形貌、化学成分、结晶度、光学性质和等温行为进行了表征。紫外可见吸收带在 365 纳米处,X 射线衍射分析证实了氧化锌氮氧化物的结晶性,颗粒大小在 32-68 纳米之间。傅立叶变换红外光谱波段证实了生物活性化合物的存在。扫描电镜图像显示形成了六角形和棒状的 NPs。研究结果表明,合成的 ZnO NPs 的形状对去除水中的 MO 有很大影响。结果表明,在 pH 值为 5 时,0.05 克的 ZnO NPs 对 MO 的去除率最高可达 68%。 这项研究展示了一种制备各种 ZnO NPs 的绿色方法,对 MO 染料的去除具有显著效果。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Green synthesis of zinc oxide nanoparticles from Salvadora persica leaf extract: Characterization and studying methyl orange removal by adsorption
The present study conducted a successful green synthesis of zinc oxide nanoparticles (ZnO NPs) from the aqueous solution of Salvadora persica leaf extract as a capping agent. The environmental application of the synthesized ZnO NP was understood from the methyl orange (MO) dye removal investigation. The morphology, chemical composition, crystallinity, optical property, and isothermal behaviour of synthesized NPs were characterized by scanning electron microscopy (SEM), energy-dispersive spectroscopy, Fourier transform infrared (FTIR), X-ray diffraction (XRD), and UV-visible spectroscopy (UV-Vis). The UV-Vis absorption band was found at 365 nm, and the XRD analysis confirmed the crystallinity of the ZnO NP and the particle sizes were in the range of 32–68 nm. The FTIR bands confirm the presence of bioactive compounds. SEM images showed the formation of hexagonal and rod-shaped NPs. The findings suggested that the shape of the synthesized ZnO NPs has a major influence on the removal of MO from water. The results revealed that a maximum MO removal of 68% was obtained with an amount of 0.05 g of ZnO NPs at pH 5. This research demonstrates a green method of preparing various ZnO NPs with a remarkable efficiency towards the removal of MO dye.
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