一步合成 ZnO、WO3 和 rGO 纳米粒子增强抗微生物活性的研究以及用于肌电图生物医学应用的 rGO 纳米电极的制造

K. Subramaniam, Konganapuram S. Mohan, Rajappan K. Bhoopesh, K.V. Gunavathy
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引用次数: 0

摘要

本研究旨在利用简单有效的化学还原技术合成 ZnO、WO3 和 rGO 纳米粒子(NPs),并研究其生物医学应用。根据 XRD 结果,合成的 NPs 具有六方、单斜和立方晶型。FESEM 显微图像显示 rGO NPs 呈片状结构,ZnO 呈海藻晶体结构,而 WO3 NPs 则呈块状团簇结构。发现 ZnO、WO3 和 rGO NPs 的带隙值分别为 5.75、5.37 和 3.01 eV。利用傅立叶变换红外光谱验证了所制备的 NPs 中存在不同的官能团。针对不同微生物的研究表明,ZnO 和 WO3 NPs 的抗菌活性有所提高。研究人员制作了涂有 rGO NP 的电极,发现它能更有效地收集人体生物医学数据。使用肌电图分析开发板和用于监测目的的安卓应用程序比较了涂有 rGO NP 的电极的性能。据观察,信号质量、信号与背景噪声之间的比率以及电极与皮肤之间的阻抗水平均优于传统电极。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Investigations on the enhanced anti-microbial activity of one step synthesized ZnO, WO3, and rGO nano particles and fabrication of rGO nano electrode for EMG biomedical application
The proposed study aims to synthesize ZnO, WO3, and rGO nano particles (NPs) using simple and effective chemical reduction technique and to investigate its biomedical applications. According to the XRD results, synthesized NPs had hexagonal, monoclinic, and cubic crystal forms. The FESEM micro image shows sheet-like structure for rGO NPs, an algal crystal structure for ZnO, and a bulk cluster formation for WO3 NPs. The value of band gap was found to be 5.75, 5.37 and 3.01 eV for ZnO, WO3, and rGO NPs respectively. The presence of diverse functional groups in the produced NPs was verified using Fourier-transform infrared spectroscopy. Investigations against different microorganisms indicated an augmentation in the antibacterial activity for ZnO and WO3 NPs. Electrodes coated with rGO NP were made and discovered to be effective in collecting human biomedical data more effectively. The performance of rGO NP coated electrodes was compared using a development board for electromyography analysis along with an android application for monitoring purposes. The quality of the signal, the ratio between the signal and the background noise, as well as the level of impedance between the electrode and the skin was observed to be better than conventional electrodes.
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