{"title":"利用 X 射线 CT 成像定量分析孔隙形态对 CP-Ti L-PBF 材料拉伸性能的影响","authors":"Yuji Shigeta, Naoyuki Nomura, Katsuyoshi Kondoh, Kentaro Uesugi, Masato Hoshino, Masatoshi Aramaki, Yukiko Ozaki","doi":"10.2355/isijinternational.isijint-2023-431","DOIUrl":null,"url":null,"abstract":"</p><p>Controlling the shape, size, and arrangement of residual defects (pores) in additive-manufactured materials is essential for improving their strength and reliability. However, quantifying the shape and arrangement of individual pores in such materials remains a challenge. This study aimed to clarify the effect of pore configurations that determine the tensile properties of laser powder-based fusion (L-PBF) materials. First, the 3D pore-configurations of pure titanium L-PBF materials fabricated under different beam energy densities were visualized using high-intensity X-ray computed tomography (CT). Subsequently, the porosity, volume equivalent diameter, and sphericity of each pore were quantified by 3D analysis of each CT image, and their correlations with the tensile properties were analyzed. The results showed that, unlike conventional sintered materials, the 0.2% yield stress did not correlate with the porosity of the specimen, suggesting heterogeneity in the hydrostatic component of stress acting on pores. This was connected to periodic fluctuation in the local porosity of the layers sliced perpendicular to the building direction. Furthermore, for specimens fabricated under relatively low beam energy densities, the porosity of the lowest density sliced layer was negatively correlated with tensile strength and total elongation, whereby the local low-density layer dominated the tensile properties. For specimens fabricated under the high energy densities where keyholes were generated, the maximum pore diameter rather than the local layer porosity was more predominate. Thus, it is evident that local structures such as local low-density regions or larger pores dominate the ductile properties of Ti L-PBF materials in terms of their tensile properties.</p>\n<p></p>","PeriodicalId":14619,"journal":{"name":"Isij International","volume":"27 1","pages":""},"PeriodicalIF":1.8000,"publicationDate":"2024-03-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Use of X-ray CT imaging to quantitatively analyze the effects of the pore morphology on the tensile properties of CP-Ti L-PBF materials\",\"authors\":\"Yuji Shigeta, Naoyuki Nomura, Katsuyoshi Kondoh, Kentaro Uesugi, Masato Hoshino, Masatoshi Aramaki, Yukiko Ozaki\",\"doi\":\"10.2355/isijinternational.isijint-2023-431\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"</p><p>Controlling the shape, size, and arrangement of residual defects (pores) in additive-manufactured materials is essential for improving their strength and reliability. However, quantifying the shape and arrangement of individual pores in such materials remains a challenge. This study aimed to clarify the effect of pore configurations that determine the tensile properties of laser powder-based fusion (L-PBF) materials. First, the 3D pore-configurations of pure titanium L-PBF materials fabricated under different beam energy densities were visualized using high-intensity X-ray computed tomography (CT). Subsequently, the porosity, volume equivalent diameter, and sphericity of each pore were quantified by 3D analysis of each CT image, and their correlations with the tensile properties were analyzed. The results showed that, unlike conventional sintered materials, the 0.2% yield stress did not correlate with the porosity of the specimen, suggesting heterogeneity in the hydrostatic component of stress acting on pores. This was connected to periodic fluctuation in the local porosity of the layers sliced perpendicular to the building direction. Furthermore, for specimens fabricated under relatively low beam energy densities, the porosity of the lowest density sliced layer was negatively correlated with tensile strength and total elongation, whereby the local low-density layer dominated the tensile properties. For specimens fabricated under the high energy densities where keyholes were generated, the maximum pore diameter rather than the local layer porosity was more predominate. 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引用次数: 0
摘要
控制添加剂制造材料中残留缺陷(孔隙)的形状、大小和排列对于提高其强度和可靠性至关重要。然而,量化此类材料中单个孔隙的形状和排列仍是一项挑战。本研究旨在阐明决定激光粉末基熔融(L-PBF)材料拉伸性能的孔隙配置的影响。首先,使用高强度 X 射线计算机断层扫描(CT)观察了在不同光束能量密度下制造的纯钛 L-PBF 材料的三维孔隙结构。随后,通过对每张 CT 图像进行三维分析,量化了每个孔隙的孔隙率、体积当量直径和球度,并分析了它们与拉伸性能的相关性。结果表明,与传统烧结材料不同,0.2%屈服应力与试样的孔隙率并不相关,这表明作用在孔隙上的静水压力成分具有异质性。这与垂直于建筑方向的切片层局部孔隙率的周期性波动有关。此外,对于在相对较低的梁能量密度下制作的试样,最低密度切片层的孔隙率与拉伸强度和总伸长率呈负相关,即局部低密度层主导了拉伸特性。在高能量密度下制作的试样会产生键孔,最大孔径比局部层孔隙率更重要。由此可见,在钛 L-PBF 材料的韧性特性中,局部结构(如局部低密度区域或较大的孔隙)在拉伸特性方面占主导地位。
Use of X-ray CT imaging to quantitatively analyze the effects of the pore morphology on the tensile properties of CP-Ti L-PBF materials
Controlling the shape, size, and arrangement of residual defects (pores) in additive-manufactured materials is essential for improving their strength and reliability. However, quantifying the shape and arrangement of individual pores in such materials remains a challenge. This study aimed to clarify the effect of pore configurations that determine the tensile properties of laser powder-based fusion (L-PBF) materials. First, the 3D pore-configurations of pure titanium L-PBF materials fabricated under different beam energy densities were visualized using high-intensity X-ray computed tomography (CT). Subsequently, the porosity, volume equivalent diameter, and sphericity of each pore were quantified by 3D analysis of each CT image, and their correlations with the tensile properties were analyzed. The results showed that, unlike conventional sintered materials, the 0.2% yield stress did not correlate with the porosity of the specimen, suggesting heterogeneity in the hydrostatic component of stress acting on pores. This was connected to periodic fluctuation in the local porosity of the layers sliced perpendicular to the building direction. Furthermore, for specimens fabricated under relatively low beam energy densities, the porosity of the lowest density sliced layer was negatively correlated with tensile strength and total elongation, whereby the local low-density layer dominated the tensile properties. For specimens fabricated under the high energy densities where keyholes were generated, the maximum pore diameter rather than the local layer porosity was more predominate. Thus, it is evident that local structures such as local low-density regions or larger pores dominate the ductile properties of Ti L-PBF materials in terms of their tensile properties.
期刊介绍:
The journal provides an international medium for the publication of fundamental and technological aspects of the properties, structure, characterization and modeling, processing, fabrication, and environmental issues of iron and steel, along with related engineering materials.