共沉淀法制备的纯 ZnO 纳米粒子和掺铜 ZnO 纳米粒子的光催化降解能力增强

IF 1 4区 材料科学
V. Balasubramanian, R. Jeyachitra, T. S. Senthil, S. Kalpana
{"title":"共沉淀法制备的纯 ZnO 纳米粒子和掺铜 ZnO 纳米粒子的光催化降解能力增强","authors":"V. Balasubramanian, R. Jeyachitra, T. S. Senthil, S. Kalpana","doi":"10.15251/jor.2024.201.103","DOIUrl":null,"url":null,"abstract":"The key goal of this study is to innovate the pure and 0.05, 0.10 and 0.15 wt.% of Cudoped ZnO NPs through co-precipitation technique. PXRD pattern shows the hexagonal crystal structure with no any phase impurity were observed for all the synthesized samples. From UV-Vis DRS spectra, band gap was obtained as 3.18, 3.24, 3.29 and 3.33 eV respectively for undoped, Cu-doped ZnO NPs (0.05, 0.10 and 0.15 wt.%). From SEM analysis, the agglomeration of rod-like morphology for pure ZnO NPs, spherical-like morphology for Cu-doped ZnO NPs (0.05 wt.%) and flake-like morphology for Cu-doped ZnO NPs (0.10 wt.%) and flower-like morphology for Cu-doped ZnO NPs (0.15 wt.%). The photocatalytic performance of the synthesized NPs was studied by the dye degradation of Methylene Blue (MB) under UV irradiation. The result exposed that, 0.15 wt.% of Cu-doped ZnO NPs is found to have efficient degradation candidate materials.","PeriodicalId":54394,"journal":{"name":"Journal of Ovonic Research","volume":"84 2","pages":""},"PeriodicalIF":1.0000,"publicationDate":"2024-02-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Enhanced photocatalytic degradation of pure and Cu-doped ZnO nanoparticles prepared under Co-precipitation method\",\"authors\":\"V. Balasubramanian, R. Jeyachitra, T. S. Senthil, S. Kalpana\",\"doi\":\"10.15251/jor.2024.201.103\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The key goal of this study is to innovate the pure and 0.05, 0.10 and 0.15 wt.% of Cudoped ZnO NPs through co-precipitation technique. PXRD pattern shows the hexagonal crystal structure with no any phase impurity were observed for all the synthesized samples. From UV-Vis DRS spectra, band gap was obtained as 3.18, 3.24, 3.29 and 3.33 eV respectively for undoped, Cu-doped ZnO NPs (0.05, 0.10 and 0.15 wt.%). From SEM analysis, the agglomeration of rod-like morphology for pure ZnO NPs, spherical-like morphology for Cu-doped ZnO NPs (0.05 wt.%) and flake-like morphology for Cu-doped ZnO NPs (0.10 wt.%) and flower-like morphology for Cu-doped ZnO NPs (0.15 wt.%). The photocatalytic performance of the synthesized NPs was studied by the dye degradation of Methylene Blue (MB) under UV irradiation. The result exposed that, 0.15 wt.% of Cu-doped ZnO NPs is found to have efficient degradation candidate materials.\",\"PeriodicalId\":54394,\"journal\":{\"name\":\"Journal of Ovonic Research\",\"volume\":\"84 2\",\"pages\":\"\"},\"PeriodicalIF\":1.0000,\"publicationDate\":\"2024-02-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Ovonic Research\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.15251/jor.2024.201.103\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Ovonic Research","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.15251/jor.2024.201.103","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

本研究的主要目标是通过共沉淀技术,创新性地合成纯度为 0.05、0.10 和 0.15 wt.% 的掺柘氧化锌纳米粒子。PXRD 图显示,所有合成样品均为六方晶体结构,无任何杂质。紫外可见 DRS 光谱显示,未掺杂、掺铜 ZnO NPs(0.05、0.10 和 0.15 wt.%)的带隙分别为 3.18、3.24、3.29 和 3.33 eV。从 SEM 分析来看,纯 ZnO NPs 呈棒状团聚,掺铜 ZnO NPs(0.05 wt.%)呈球状团聚,掺铜 ZnO NPs(0.10 wt.%)呈片状团聚,掺铜 ZnO NPs(0.15 wt.%)呈花状团聚。在紫外线照射下,通过降解染料亚甲基蓝(MB)研究了合成氮氧化物的光催化性能。结果表明,0.15 wt.% 的掺铜氧化锌 NPs 是高效的降解候选材料。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Enhanced photocatalytic degradation of pure and Cu-doped ZnO nanoparticles prepared under Co-precipitation method
The key goal of this study is to innovate the pure and 0.05, 0.10 and 0.15 wt.% of Cudoped ZnO NPs through co-precipitation technique. PXRD pattern shows the hexagonal crystal structure with no any phase impurity were observed for all the synthesized samples. From UV-Vis DRS spectra, band gap was obtained as 3.18, 3.24, 3.29 and 3.33 eV respectively for undoped, Cu-doped ZnO NPs (0.05, 0.10 and 0.15 wt.%). From SEM analysis, the agglomeration of rod-like morphology for pure ZnO NPs, spherical-like morphology for Cu-doped ZnO NPs (0.05 wt.%) and flake-like morphology for Cu-doped ZnO NPs (0.10 wt.%) and flower-like morphology for Cu-doped ZnO NPs (0.15 wt.%). The photocatalytic performance of the synthesized NPs was studied by the dye degradation of Methylene Blue (MB) under UV irradiation. The result exposed that, 0.15 wt.% of Cu-doped ZnO NPs is found to have efficient degradation candidate materials.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Journal of Ovonic Research
Journal of Ovonic Research Materials Science-Electronic, Optical and Magnetic Materials
CiteScore
1.60
自引率
20.00%
发文量
77
期刊介绍: Journal of Ovonic Research (JOR) appears with six issues per year and is open to the reviews, papers, short communications and breakings news inserted as Short Notes, in the field of ovonic (mainly chalcogenide) materials for memories, smart materials based on ovonic materials (combinations of various elements including chalcogenides), materials with nano-structures based on various alloys, as well as semiconducting materials and alloys based on amorphous silicon, germanium, carbon in their various nanostructured forms, either simple or doped/alloyed with hydrogen, fluorine, chlorine and other elements of high interest for applications in electronics and optoelectronics. Papers on minerals with possible applications in electronics and optoelectronics are encouraged.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信