"Datura metel 叶提取物对 Cd@ZnO NCs 减少污染物和抗菌活性的影响

IF 2.218 Q2 Chemistry
Prathap A , H.S.Bhojya Naik , R. Viswanath
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引用次数: 0

摘要

本研究采用共沉淀法,在不改变掺杂剂浓度的情况下,利用大杜拉叶提取物合成了镉@氧化锌(x=0,5,15 ml)纳米复合材料(NCs),并对其物理和光学特性进行了比较。对其进行了紫外可见光、傅立叶变换红外光谱、PXRD、FESEM、EDAX、HRTEM、拉曼光谱和 PL 分析。PXD 证实了纯净的 FCC 结晶,晶粒大小分别为 32.35、27.82 和 27.51 nm。傅立叶变换红外光谱证实,植物前驱体在 546、507、487 和 433cm-1 处的伸展振动起到了还原剂和封端剂的作用。SEM 和 HRTEM 数据显示,纳米复合材料呈球形,颗粒大小几乎相同。EDAX 显示存在镉 @ 氧化锌(x=0,5,15 ml)纳米复合材料。拉曼光谱显示,Cd@ZnO NCs 呈六方晶系(菱锌结构)。光致发光光谱中观察到一个蓝色发射峰。紫外可见光谱测定了合成纳米复合材料的带隙。g-CZO 纳米复合材料有效地控制了金黄色葡萄球菌和肺炎克雷伯氏菌这两种细菌的抗菌活性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
“Effect of datura metel leaf extract on Cd@ZnO NCs for pollutant reduction and antimicrobial activity”

This work reports a facile approach for synthesizing Cadmium @ Zinc oxide (x = 0, 5, 15 ml) nanocomposites (NCs) using leaf extracts of datura by co-precipitation method without varying the concentration of dopant followed by the comparison of their physical and optical properties. It is characterized by UV–vis, FTIR, PXRD, FESEM, EDAX, HRTEM, Raman spectroscopy, and PL analysis. PXD confirmed pure and crystallized with FCC with 32.35, 27.82, and 27.51 nm grain sizes. FTIR confirms that plant precursors acted as reducing and capping agents by stretching vibration at 546, 507, 487, and 433cm−1. SEM and HRTEM data revealed the existence of spherical nanocomposites with nearly identical particle sizes. EDAX showed the existence of a nanocomposite of Cadmium @ Zinc oxide (x = 0, 5, 15 ml) nanocomposite. Raman spectra indicated that the Cd@ZnO NCs were crystallized in a hexagonal (wurtzite structure). A blue emission peak was observed in photoluminescence spectra. In the UV–Vis spectroscopy, band gaps of the synthesized nanocomposite are determined. By increasing extraction concentrations, the degradation efficiency of rhodamine-B dye increases up to 87.87 %. g-CZO nanocomposite effectively controlled both bacterial species Staphylococcus aureus and Klebsiella pneumonia in antimicrobial activity.

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来源期刊
Chemical Data Collections
Chemical Data Collections Chemistry-Chemistry (all)
CiteScore
6.10
自引率
0.00%
发文量
169
审稿时长
24 days
期刊介绍: Chemical Data Collections (CDC) provides a publication outlet for the increasing need to make research material and data easy to share and re-use. Publication of research data with CDC will allow scientists to: -Make their data easy to find and access -Benefit from the fast publication process -Contribute to proper data citation and attribution -Publish their intermediate and null/negative results -Receive recognition for the work that does not fit traditional article format. The research data will be published as ''data articles'' that support fast and easy submission and quick peer-review processes. Data articles introduced by CDC are short self-contained publications about research materials and data. They must provide the scientific context of the described work and contain the following elements: a title, list of authors (plus affiliations), abstract, keywords, graphical abstract, metadata table, main text and at least three references. The journal welcomes submissions focusing on (but not limited to) the following categories of research output: spectral data, syntheses, crystallographic data, computational simulations, molecular dynamics and models, physicochemical data, etc.
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