{"title":"在 XRD 研究之前从粘性和非挥发性溶剂中清洗重结晶药物的简单策略：技术说明","authors":"E. Rahimpour, A. Jouyban","doi":"10.15446/rcciquifa.v52n1.109364","DOIUrl":null,"url":null,"abstract":"Aim: obtaining a dried powder residual from a viscous and non-volatile solvents isimpossible. Thus, their analysis by using the methods required for the dried formof materials has always been a problem. In the current technical note, our aim wasto offer a simple method for this issue. Results: the proposed method was basedon washing of the viscous residuals with a volatile solvent and their drying in theambient conditions. For this purpose, we have provided sufficient data on somedrugs in the selected viscous and non-volatile solvents to support our claim.","PeriodicalId":21220,"journal":{"name":"Revista Colombiana de Ciencias Químico-Farmacéuticas","volume":"35 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2023-07-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"A simple strategy for washing a recrystallized drug from viscous and non-volatile solvents prior to XRD study: A technical note\",\"authors\":\"E. Rahimpour, A. Jouyban\",\"doi\":\"10.15446/rcciquifa.v52n1.109364\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Aim: obtaining a dried powder residual from a viscous and non-volatile solvents isimpossible. Thus, their analysis by using the methods required for the dried formof materials has always been a problem. In the current technical note, our aim wasto offer a simple method for this issue. Results: the proposed method was basedon washing of the viscous residuals with a volatile solvent and their drying in theambient conditions. For this purpose, we have provided sufficient data on somedrugs in the selected viscous and non-volatile solvents to support our claim.\",\"PeriodicalId\":21220,\"journal\":{\"name\":\"Revista Colombiana de Ciencias Químico-Farmacéuticas\",\"volume\":\"35 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-07-24\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Revista Colombiana de Ciencias Químico-Farmacéuticas\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.15446/rcciquifa.v52n1.109364\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Revista Colombiana de Ciencias Químico-Farmacéuticas","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.15446/rcciquifa.v52n1.109364","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
A simple strategy for washing a recrystallized drug from viscous and non-volatile solvents prior to XRD study: A technical note
Aim: obtaining a dried powder residual from a viscous and non-volatile solvents isimpossible. Thus, their analysis by using the methods required for the dried formof materials has always been a problem. In the current technical note, our aim wasto offer a simple method for this issue. Results: the proposed method was basedon washing of the viscous residuals with a volatile solvent and their drying in theambient conditions. For this purpose, we have provided sufficient data on somedrugs in the selected viscous and non-volatile solvents to support our claim.
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