从甘蔗渣中合成醋酸纤维素作为生物降解泡沫原材料

Meidini Suci Anjarwati, Anerasari Meidinariasty, Muhammad Yerizam
{"title":"从甘蔗渣中合成醋酸纤维素作为生物降解泡沫原材料","authors":"Meidini Suci Anjarwati, Anerasari Meidinariasty, Muhammad Yerizam","doi":"10.32672/jse.v8i4.5893","DOIUrl":null,"url":null,"abstract":"The high cellulose content of bagasse allows it to be developed into a variety of valuable products, one of them is cellulose acetate which will be used to make biodegradable foam. The purpose of this research is to determine the best conditions for the synthesis of cellulose acetate from bagasse and test how cellulose acetate can be used to make biodegradable foam. This study used phosphoric acid as a solvent and glacial acetic acid as an acetylating agent to make cellulose acetate through the acetylation process. The variations in acetylation time in this study were 15, 30, and 45 minutes and the volume of glacial acetic acid as acetylating agent was 20, 40, 60, 80, and 100 ml. The results of this study indicated that the optimum conditions for the synthesis of cellulose acetate are 15 minutes of acetylation with a volume of 100 ml of glacial acetic acid, with a yield of 79.31% cellulose acetate, 36.19% acetyl content and a degree of substitution of 2.11. The test for the application of cellulose acetate to make biodegradable foam obtained a water absorption of 18.81%, the biodegradation test obtained was 24.53% in 14 days. In the biodegradable foam leak test for 10 minutes, no leakage occurred. This indicated that the biodegradable foam obtained was suitable to use because it complied with SNI.","PeriodicalId":17758,"journal":{"name":"Jurnal Serambi Engineering","volume":"54 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2023-10-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Sintesis Selulosa Asetat dari Ampas Tebu sebagai Bahan Baku Biodegradable Foam\",\"authors\":\"Meidini Suci Anjarwati, Anerasari Meidinariasty, Muhammad Yerizam\",\"doi\":\"10.32672/jse.v8i4.5893\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The high cellulose content of bagasse allows it to be developed into a variety of valuable products, one of them is cellulose acetate which will be used to make biodegradable foam. The purpose of this research is to determine the best conditions for the synthesis of cellulose acetate from bagasse and test how cellulose acetate can be used to make biodegradable foam. This study used phosphoric acid as a solvent and glacial acetic acid as an acetylating agent to make cellulose acetate through the acetylation process. The variations in acetylation time in this study were 15, 30, and 45 minutes and the volume of glacial acetic acid as acetylating agent was 20, 40, 60, 80, and 100 ml. The results of this study indicated that the optimum conditions for the synthesis of cellulose acetate are 15 minutes of acetylation with a volume of 100 ml of glacial acetic acid, with a yield of 79.31% cellulose acetate, 36.19% acetyl content and a degree of substitution of 2.11. The test for the application of cellulose acetate to make biodegradable foam obtained a water absorption of 18.81%, the biodegradation test obtained was 24.53% in 14 days. In the biodegradable foam leak test for 10 minutes, no leakage occurred. This indicated that the biodegradable foam obtained was suitable to use because it complied with SNI.\",\"PeriodicalId\":17758,\"journal\":{\"name\":\"Jurnal Serambi Engineering\",\"volume\":\"54 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-10-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Jurnal Serambi Engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.32672/jse.v8i4.5893\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Jurnal Serambi Engineering","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.32672/jse.v8i4.5893","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

甘蔗渣的纤维素含量很高,可将其开发成各种有价值的产品,醋酸纤维素就是其中之一,它将用于制造可生物降解的泡沫塑料。本研究的目的是确定从甘蔗渣中合成醋酸纤维素的最佳条件,并测试如何利用醋酸纤维素制造可生物降解的泡沫塑料。本研究以磷酸为溶剂,冰醋酸为乙酰化剂,通过乙酰化过程制得乙酸纤维素。乙酰化时间分别为 15 分钟、30 分钟和 45 分钟,乙酰化剂冰醋酸的用量分别为 20 毫升、40 毫升、60 毫升、80 毫升和 100 毫升。研究结果表明,合成乙酸纤维素的最佳条件是乙酰化时间为 15 分钟,冰醋酸体积为 100 毫升,乙酸纤维素的产率为 79.31%,乙酰含量为 36.19%,取代度为 2.11。应用醋酸纤维素制作可生物降解泡沫的测试结果是,吸水率为 18.81%,14 天后的生物降解率为 24.53%。在 10 分钟的可生物降解泡沫泄漏试验中,没有发生泄漏。这表明获得的生物降解泡沫符合 SNI 标准,可以使用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Sintesis Selulosa Asetat dari Ampas Tebu sebagai Bahan Baku Biodegradable Foam
The high cellulose content of bagasse allows it to be developed into a variety of valuable products, one of them is cellulose acetate which will be used to make biodegradable foam. The purpose of this research is to determine the best conditions for the synthesis of cellulose acetate from bagasse and test how cellulose acetate can be used to make biodegradable foam. This study used phosphoric acid as a solvent and glacial acetic acid as an acetylating agent to make cellulose acetate through the acetylation process. The variations in acetylation time in this study were 15, 30, and 45 minutes and the volume of glacial acetic acid as acetylating agent was 20, 40, 60, 80, and 100 ml. The results of this study indicated that the optimum conditions for the synthesis of cellulose acetate are 15 minutes of acetylation with a volume of 100 ml of glacial acetic acid, with a yield of 79.31% cellulose acetate, 36.19% acetyl content and a degree of substitution of 2.11. The test for the application of cellulose acetate to make biodegradable foam obtained a water absorption of 18.81%, the biodegradation test obtained was 24.53% in 14 days. In the biodegradable foam leak test for 10 minutes, no leakage occurred. This indicated that the biodegradable foam obtained was suitable to use because it complied with SNI.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信