罂粟(Amorphophallus oncophyllus)的抗溶解性和防腐性的提高。

Fikratul Ihsan, Anna Anggraini, Hanifah Ulfa Azzahro
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引用次数: 0

摘要

以葡甘聚糖形式出口的茯苓块茎比薯片更有经济价值。葡甘露聚糖是一种水溶性纤维,可使用极性溶剂进行提取,也可使用非极性反溶剂进行沉淀。选择最佳提取时间和使用抗溶剂比例可以提高葡甘露聚糖的产量。所使用的反溶剂异丙醇(IPA)的介电常数比乙醇低,因此非极性更强。本研究的目的是结合萃取时间处理和作为反溶剂的异丙醇的比例来获得最佳产量。采用的设计是随机完全因子设计(RALF),有两个水平,即提取时间(1、2 和 3 小时)和茯苓粉与异丙醇的比例(1:10、1:15 和 1:20)。结果表明,提取时间与异丙醇反溶剂比例的交互作用对葡甘露聚糖的产量有显著影响。2 小时提取时间与反溶剂比例(1:15)的交互作用产生了最好的葡甘露聚糖产量,即 66.69%。茯苓粉的傅立叶变换红外光谱检测结果和葡甘聚糖提取结果显示,每个振动的波数都发生了变化,尤其是在指纹区。在波数 806.25 cm-1 和 875.68 cm-1 处检测到了葡甘聚糖提取过程中产生的 β-糖苷键和 β-甘露糖苷键的 C-H 振动。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
EKSTRAKSI GLUKOMANAN DARI TEPUNG PORANG (Amorphophallus oncophyllus) DENGAN KOMBINASI PERLAKUAN WAKTU EKSTRAKSI DAN ANTI-SOLVENT
Exports of porang tubers form glucomannan are more economically valuable than form of chips. Glucomannan is a water-soluble fiber that can be extracted using polar solvents and precipitated using non-polar anti-solvents. Selecting the best extraction time and using the anti-solvent ratio could increased the yield of glucomannan. The used of anti-solvent Isopropyl alcohol (IPA) had a lower dielectric constant compared to ethanol, so it is more non-polar. An aim of this research was to obtain the best yield from a combination of extraction time treatment and the ratio of IPA as anti-solvent. The design used was a randomized complete factorial design (RALF) with two levels that is extraction time (1, 2 and 3 hours) and the ratio of porang flour to isopropyl alcohol (1:10, 1:15 and 1:20). The results showed that the interaction of extraction time and IPA anti-solvent ratio had a significant effect on the yield of glucomannan. The interaction of the 2 hour extraction time treatment with the anti-solvent ratio (1:15) produced the best glucomannan yield that is 66.69%. The results of FTIR testing of porang flour and glucomannan extraction results showed a shift in the wave number for each vibration, especially in the fingerprint area. C-H vibrations from β-glycosidic and β-manosidic bonds resulting from glucomannan extraction were detected at wave numbers 806.25 cm-1 and 875.68 cm-1.
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