Durometric analysis of hardening of the near-surface layer of ADI during friction at the influence of the TRIP effect

Features of strengthening of the near-surface layer of ADI during friction due to strain-induced martensitic transformation were analyzed by duromeric methods. Indentation under continuous loading (Meyer hardness, HM) and Vickers microhardness Hμ were used. Pop–ins are observed on the ADI continuous load curves, which indicate martensitic transformations during indentation. The effect usually exists at a load of ~0,1 H and an depth of ~1,5 μk. The average microhardness of the initial sample is Hμ ≈ 4,89 GPa. After wear, the average value increases to Hμ ≈ 6,92 GPa. Statistical analysis of the microhardness distribution of the sample after wear revealed that a third of the indentations have abnormally high hardness, which is characteristic of deformation-induced martensite. Probably, these indents are obtained from regions of the structure where deformation-induced martensitic transformation took place. Increasing the indentation load practically does not affect the determination of the microhardness of the initial sample, but reduces the hardness of the sample after wear. This indicates the gradient nature of deformation and phase-structural rearrangements in the near-surface layer during wear. As the friction temperature increases, there is a decrease in microhardness in the wear zone. This is explained by the departure from the temperature range of the martensitic transformation, due to which the TRIP effect is weakened. The maximum degradation of microhardness is observed between room temperature and 50 oC. Keywords: ADI materials, durometric studies, TRIP-effect, wear.