热循环对纳米杂化和高粘度松散填充树脂基复合材料表面粗糙度的影响

Ryta Łagocka, Mateusz Granat, Katarzyna Lewusz-Butkiewicz, M. Tomasik, M. Lipski
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摘要

摘要 引言:本研究旨在研究热循环对高粘度树脂基复合材料(RBC)表面几何形状的影响,并与传统的纳米混合复合材料进行比较。材料与方法测试了四种传统纳米混合复合材料(Tetric EvoCeram - TEC、GrandioSO - GD、Filtek Z550 - FZ 和 Ceram-X Mono - CX)和四种高粘度填充复合材料(Tetric EvoCeram Bulk Fill - TBF、X-tra fil - XF、Filtek Bulk Fill Posterior - FBF 和 QuixFil - QF)。经过两步抛光程序后,样品被分为两组:对照组(K)和热循环组(TC)。TC 组样品按照 ISO 11405 标准进行热循环(THE-1100,SD Mechatronik GmbH)。表面几何形状由轮廓仪(Turbowave v. 7.36,Hommel-Etamic)和扫描电子显微镜 - SEM(VEGA 3,Tescan Analytics)进行评估。结果:热循环增加了传统 RBC 的表面粗糙度:TEC(p = 0.000007)、GD(p = 0.04)和 CX(p = 0.0005)。散装填充复合材料的表面粗糙度有所降低:XF (p = 0.000003) 和 QF (p = 0.0002)。热循环改变了 TEC、CX、XF 和 QF 材料的表面粗糙度。结论根据 ISO 11405 标准,在水环境中进行热循环会导致有机基质降解,并使传统和高粘度松散填料复合材料表面的填料分子暴露出来。一些经过测试的 RBC,尤其是含有现代疏水单体的 RBC,不太容易受到这些过程的影响。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
The effect of thermal cycling on the surface roughness of nanohybrid and high-viscosity bulk-fill resin-based composites
Abstract Introduction: The aim of this study was to investigate the effect of thermal cycling on the surface geometry of high-viscosity bulk-fill resin-based composites (RBCs) compared to conventional nanohybrid composites. Materials and methods: Four conventional nanohybrid composites (Tetric EvoCeram – TEC, GrandioSO – GD, Filtek Z550 – FZ, and Ceram·X Mono – CX) and 4 high-viscosity bulk-fill composites (Tetric EvoCeram Bulk Fill – TBF, X-tra fil – XF, Filtek Bulk Fill Posterior – FBF, and QuixFil – QF) were tested. After the 2-step polishing procedure, the samples were divided into 2 groups: control group (K) and thermal cycling group (TC). Samples from the TC were subjected to thermal cycling according to ISO 11405 (THE-1100, SD Mechatronik GmbH). Surface geometry was evaluated by profilometry (Turbowave v. 7.36, Hommel-Etamic) and scanning electron microscope – SEM (VEGA 3, Tescan Analytics). Results: The applied thermal cycles increased the surface roughness of conventional RBCs: TEC (p = 0.000007), GD (p = 0.04), and CX (p = 0.0005). A reduction in the surface roughness of bulk-fill composites was observed in the case of materials: XF (p = 0.000003) and QF (p = 0.0002). Thermal cycling was shown to alter the surface roughness of the TEC, CX, XF, and QF materials. Conclusion: The application of thermal cycling in a water environment in accordance with the ISO 11405 standard causes the degradation of the organic matrix and the exposure of filler molecules on the surface of both conventional and high-viscosity bulk-fill composites. Some of the tested RBCs, especially those containing modern hydrophobic monomers, are less susceptible to these processes.
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