哈塔伊省采集的牛肉中土霉素和恩诺沙星残留量调查

Özlem ÇİÇEK DOĞAN, Erdinç Türk, D. Durna Corum
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引用次数: 0

摘要

研究目的本研究旨在调查从哈塔伊省不同地区采集的牛肉样本中土霉素和恩诺沙星的残留量。材料和方法:从屠夫和市场随机获取 50 份牛肉样本,每份 100 克。样品分析采用高效液相色谱法。 主要结果欧盟(EU)和土耳其食品法典(TGK)规定的红肉中恩诺沙星、环丙沙星和四环素的最高残留限量为 100 微克/千克,而联合国粮农组织(FAO)规定的最高残留限量为 200 微克/千克。在 50 个牛肉样本中,有 5 个样本(10%)发现土霉素、恩诺沙星及其代谢物环丙沙星的残留量低于技术食品委员会和粮农组织确定的最高残留限量。在 90% 的样本中,没有检测到恩诺沙星、土霉素和环丙沙星的残留。不过,在两个肌肉样本(4%)中发现恩诺沙星残余物,浓度分别为每公斤 47 微克和 57 微克,环丙沙星残余物浓度为每公斤 60 微克。此外,在两个样本(4%)中检测到土霉素残留,浓度分别为每公斤 88 微克和 95 微克。 据观察,哈塔伊省在育肥中使用土霉素和恩诺沙星,并遵守宰前等待期的规定。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Investigation of oxytetracycline and enrofloxacin residue in beef collected from Hatay province
Aim to study: This study purposed to investigate the residues of oxytetracycline and enrofloxacin in beef samples collected from different districts of Hatay province. Material and Methods: Fifty beef samples, each weighing 100 grams, were randomly acquired from butchers and markets. High-performance liquid chromatography was utilized for sample analysis. Main results: The MRL for red meat in the European Union (EU) and the Turkish Food Codex (TGK) is 100 μg/kg for enrofloxacin, ciprofloxacin and tetracycline, while according to the Food and Agriculture Organization (FAO) it is 200 μg/kg. Residues of oxytetracycline, enrofloxacin, and its metabolite ciprofloxacin were found below the maximum residue limits determined by the TFC and FAO in 5 (10%) out of 50 beef samples. In 90% of the samples, no residues of enrofloxacin, oxytetracycline, and ciprofloxacin were detected. However, enrofloxacin residues were found in 2 muscle samples (4%) at concentration of 47 µg/kg and 57 µg/kg, and ciprofloxacin residues of 60 µg/kg. Additionally, oxytetracycline residues were detected in 2 samples (4%) at concentrations of 88 μg/kg and 95 μg/kg. It was observed that oxytetracycline and enrofloxacin are used in fattening in Hatay province and pre-slaughter waiting periods are adhered to.
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