Salih Çağatay Koçak, Doğan Şimşek, İjlal Şimşek, Dursun Özyürek
{"title":"添加不同数量的合金元素并在不同时间进行陈化的 17-4 PH 不锈钢的腐蚀行为","authors":"Salih Çağatay Koçak, Doğan Şimşek, İjlal Şimşek, Dursun Özyürek","doi":"10.1134/S2070205123701174","DOIUrl":null,"url":null,"abstract":"<p>In this study the corrosion behaviour of 17-4 PH (precipitation hardening) stainless steel alloys, produced by adding Ta different amounts with the method of powder metallurgy, and aged at different times was investigated. Four different amounts tantalum (0.15, 0.30, 0.45 and 0.60% weight) was added to the alloy. The prepared powders were produced green compacts at ∅10 × 6 mm dimensions (800 MPa) after mixing with turbule for 2 hours. Green compacts produced were sintered for 1 h at 1300°C under a vacuum of 10<sup>–6</sup> mbar. The sintered samples were aged 1, 4 and 8 hours at 480°C after being in solution at 1050°C. Polarization measurements were performed in a corrosion cell, using three different electrode technique. In the corrosion tests, 0.1 M H<sub>2</sub>SO<sub>4</sub> was used as the electrolyte medium. As a result of the studies, the alloy the hardness and densities were increased with increasing Ta amount. Similarly, the hardness and densities of produced samples were with increasing aging time. The corrosion tests revealed that increasing the amount of Ta added to the alloy increased the alloy’s resistance to corrosion. The alloy’s corrosion resistance decreased as aging time increased. The active corrosion mechanism was seen to be pitting corrosion in all alloys.</p>","PeriodicalId":745,"journal":{"name":"Protection of Metals and Physical Chemistry of Surfaces","volume":"59 6","pages":"1298 - 1305"},"PeriodicalIF":1.1000,"publicationDate":"2023-12-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Corrosion Behaviour of 17-4 PH Stainless Steels Produced by Adding Different Amounts of Alloying Element and Aged at Different Times\",\"authors\":\"Salih Çağatay Koçak, Doğan Şimşek, İjlal Şimşek, Dursun Özyürek\",\"doi\":\"10.1134/S2070205123701174\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>In this study the corrosion behaviour of 17-4 PH (precipitation hardening) stainless steel alloys, produced by adding Ta different amounts with the method of powder metallurgy, and aged at different times was investigated. Four different amounts tantalum (0.15, 0.30, 0.45 and 0.60% weight) was added to the alloy. The prepared powders were produced green compacts at ∅10 × 6 mm dimensions (800 MPa) after mixing with turbule for 2 hours. Green compacts produced were sintered for 1 h at 1300°C under a vacuum of 10<sup>–6</sup> mbar. The sintered samples were aged 1, 4 and 8 hours at 480°C after being in solution at 1050°C. Polarization measurements were performed in a corrosion cell, using three different electrode technique. In the corrosion tests, 0.1 M H<sub>2</sub>SO<sub>4</sub> was used as the electrolyte medium. As a result of the studies, the alloy the hardness and densities were increased with increasing Ta amount. Similarly, the hardness and densities of produced samples were with increasing aging time. The corrosion tests revealed that increasing the amount of Ta added to the alloy increased the alloy’s resistance to corrosion. The alloy’s corrosion resistance decreased as aging time increased. The active corrosion mechanism was seen to be pitting corrosion in all alloys.</p>\",\"PeriodicalId\":745,\"journal\":{\"name\":\"Protection of Metals and Physical Chemistry of Surfaces\",\"volume\":\"59 6\",\"pages\":\"1298 - 1305\"},\"PeriodicalIF\":1.1000,\"publicationDate\":\"2023-12-29\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Protection of Metals and Physical Chemistry of Surfaces\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S2070205123701174\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"METALLURGY & METALLURGICAL ENGINEERING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Protection of Metals and Physical Chemistry of Surfaces","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1134/S2070205123701174","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"METALLURGY & METALLURGICAL ENGINEERING","Score":null,"Total":0}
引用次数: 0
摘要
摘要 在本研究中,研究了通过粉末冶金法添加不同量的 Ta 而制成的 17-4 PH(沉淀硬化)不锈钢合金在不同时间老化后的腐蚀行为。合金中添加了四种不同数量的钽(0.15、0.30、0.45 和 0.60%)。将制备好的粉末与透平混合 2 小时后,生产出尺寸为 ∅10 × 6 毫米(800 兆帕)的绿色压实物。在 10-6 毫巴的真空条件下,在 1300°C 的温度下烧结 1 小时。烧结样品在 1050°C 的溶液温度下分别在 480°C 下老化 1、4 和 8 小时。在腐蚀池中使用三种不同的电极技术进行了极化测量。在腐蚀试验中,使用了 0.1 M H2SO4 作为电解质介质。研究结果表明,合金的硬度和密度随着 Ta 量的增加而增加。同样,生产的样品的硬度和密度也随着老化时间的延长而增加。腐蚀测试表明,合金中添加的 Ta 量越多,合金的抗腐蚀性越强。随着老化时间的延长,合金的耐腐蚀性降低。所有合金的主要腐蚀机制都是点腐蚀。
Corrosion Behaviour of 17-4 PH Stainless Steels Produced by Adding Different Amounts of Alloying Element and Aged at Different Times
In this study the corrosion behaviour of 17-4 PH (precipitation hardening) stainless steel alloys, produced by adding Ta different amounts with the method of powder metallurgy, and aged at different times was investigated. Four different amounts tantalum (0.15, 0.30, 0.45 and 0.60% weight) was added to the alloy. The prepared powders were produced green compacts at ∅10 × 6 mm dimensions (800 MPa) after mixing with turbule for 2 hours. Green compacts produced were sintered for 1 h at 1300°C under a vacuum of 10–6 mbar. The sintered samples were aged 1, 4 and 8 hours at 480°C after being in solution at 1050°C. Polarization measurements were performed in a corrosion cell, using three different electrode technique. In the corrosion tests, 0.1 M H2SO4 was used as the electrolyte medium. As a result of the studies, the alloy the hardness and densities were increased with increasing Ta amount. Similarly, the hardness and densities of produced samples were with increasing aging time. The corrosion tests revealed that increasing the amount of Ta added to the alloy increased the alloy’s resistance to corrosion. The alloy’s corrosion resistance decreased as aging time increased. The active corrosion mechanism was seen to be pitting corrosion in all alloys.
期刊介绍:
Protection of Metals and Physical Chemistry of Surfaces is an international peer reviewed journal that publishes articles covering all aspects of the physical chemistry of materials and interfaces in various environments. The journal covers all related problems of modern physical chemistry and materials science, including: physicochemical processes at interfaces; adsorption phenomena; complexing from molecular and supramolecular structures at the interfaces to new substances, materials and coatings; nanoscale and nanostructured materials and coatings, composed and dispersed materials; physicochemical problems of corrosion, degradation and protection; investigation methods for surface and interface systems, processes, structures, materials and coatings. No principe restrictions exist related systems, types of processes, methods of control and study. The journal welcomes conceptual, theoretical, experimental, methodological, instrumental, environmental, and all other possible studies.