浸渍介导的大麻叶油萃取及薄层色谱法分离 Δ9-Tetrahydrocannabivarin (THCV)

Shazia Zulfqar, Gul Bahar Ali, Soha Jamal, Shafqat Munir, Alia Muqqddus
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引用次数: 0

摘要

采用溶剂萃取-回流冷凝器法从大麻叶片中提取非精神活性大麻素大麻二酚(Cannabidiol, CBD)。测定了大麻二酚(CBD)的理化性质。对提取油的各项参数和含量进行了分析。通过施加不同的条件制备了两种不同的样品。样品A采用回流冷凝器制备,样品B采用乙醇(溶剂)浸泡一周制备。对提取油的各项参数和含量进行了分析。采用TLC、UV、GC-MS、IR和HPLC等技术对样品和油进行表征。还进行了蛋白质、碳水化合物、类固醇、单宁、树胶和粘液的检测。用滴定法计算酸值、皂化数和比重
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Maceration Mediated Extraction of Marijuana Leaves Oil and Separation of Δ9-Tetrahydrocannabivarin (THCV) by Thin Layer Chromatography
Cannabidiol (CBD), non-psychoactive cannabinoid, was extracted from Cannabis sativa leaves by using solvent extraction method followed by reflux condenser procedure. Physical and chemical properties of Cannabidiol (CBD) were determined. Various parameters and contents of extracted oil were analyzed. Two different samples were prepared by applying different conditions. Sample “A” was prepared by applying reflux condenser and sample “B” was prepared by soaking eaves in ethanol (solvent) for one week. Various parameters and contents of extracted oil were analyzed. TLC, UV, GC-MS, IR and HPLC techniques were applied for characterization of both samples and oil. Some tests were also performed for the detection of proteins, carbohydrates, Steroids, tannins, gums and mucilage. Acid value, saponification number and specific gravity were also calculation by applying titration method
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