由于CO2捕获而获得的三种新化合物的x射线粉末衍射数据

IF 0.3 4区材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING

Powder Diffraction Pub Date : 2023-11-23 DOI:10.1017/s0885715623000404

Klaudia Nowakowska, Wiesław Łasocha

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引用次数: 0

摘要

与二氧化碳捕获相关的研究领域对于可持续的绿色化学来说是非常重要和有吸引力的。在我们的研究中对这一主题的关注导致了以二胺为基础的新化合物的获得。由于二胺的水溶液暴露在空气中二氧化碳的缓慢作用下进行合成，得到了三种新的单氨基甲酸酯。所得化合物的x射线粉末衍射数据:12-propCO2 (C4H10N2O2) [a = 9.3033(7)， b = 9.2485(7)， c = 7.4735(7) Å， β = 111.214(7)°，V = 599.46 Å3, Z = 4，空间群Ia];13- proco2 (C4H10N2O2) [a = 5.0065(10)， b = 12.2093(23)， c = 4.9006(10) Å， β = 96.457(18)°，V = 297.65 Å3, Z = 2，空间群P21];和13-dytekCO2 (C6H14N2O2) [a = 28.374(3)， c = 5.1726(9) Å， V = 3606.53 Å3, Z = 18，空间群$R\bar{3}$]。

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X-ray powder diffraction data for three new compounds obtained as a result of CO2 capture

The field of research related to CO2 capture is significant and really attractive for sustainable green chemistry. Focusing attention on this topic in our research led to obtaining new compounds based on diamines. As a result of the syntheses carried out using aqueous solutions of diamines exposed to the slow action of carbon dioxide from the air, three new monocarbamates were obtained. X-ray powder diffraction data for the obtained compounds: 12-propCO2 (C4H10N2O2) [a = 9.3033(7), b = 9.2485(7), c = 7.4735(7) Å, β = 111.214(7)°, V = 599.46 Å3, Z = 4, space group Ia]; 13-propCO2 (C4H10N2O2) [a = 5.0065(10), b = 12.2093(23), c = 4.9006(10) Å, β = 96.457(18)°, V = 297.65 Å3, Z = 2, space group P21]; and 13-dytekCO2 (C6H14N2O2) [a = 28.374(3), c = 5.1726(9) Å, V = 3606.53 Å3, Z = 18, space group

$R\bar{3}$

] are reported in this paper.

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来源期刊

$Powder Diffraction$

Powder Diffraction 工程技术-材料科学：表征与测试

CiteScore

0.90

自引率

0.00%

发文量

审稿时长

>12 weeks

期刊介绍： Powder Diffraction is a quarterly journal publishing articles, both experimental and theoretical, on the use of powder diffraction and related techniques for the characterization of crystalline materials. It is published by Cambridge University Press (CUP) for the International Centre for Diffraction Data (ICDD).