陈皮精油负载聚乳酸基纳米纤维的制备与表征

Tuğba GÜNGÖR ERTUĞRAL, Sevim AKÇURA
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引用次数: 0

摘要

静电纺丝法是一种在高压条件下生产纳米纤维的经济方法。从天然来源获得的精油具有抗氧化、抗菌和抗真菌的特性,在电纺丝法生产纳米材料中是首选的。本研究采用水蒸气蒸馏法提取陈皮精油。气相色谱-质谱法(GS-MS)检测到的10种成分中d -柠檬烯含量最高,占比77.45。以25% TPEO和聚乳酸(PLA)为原料制备复合纳米纤维。采用扫描电镜(SEM)和热重分析(TGA)对纳米纤维进行了表征。SEM结果表明,精油在聚乳酸纳米纤维结构中复合出明显的球状结构,得到的纳米纤维直径约为76.8 nm。其分解温度约为320℃。从陈皮中提取的纳米纤维及其抗菌性能,可推荐用于食品保鲜和医药领域。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Preparation and Characterization of Polylactic Acid Based Nanofiber Loaded with Tangerine Peel (Citrus Unshiu) Essential Oil
Electrospinning method used in nanofiber production is an economical method applied with high voltage electricity.Essential oils obtained from natural sources have antioxidant, antimicrobial and antifungal properties and are preferred in the production of nanomaterials by electro-spinning method. In this study, tangerine peel (citrus unshiu) essential oil (TPEO) was obtained by hydro-distillation method. The major one of the 10 components of the extract detected by Gas Chromatography Mass Spectrometry (GS-MS) was D-Limonene (%77.45). The composite nanofiber was prepared with 25% TPEO and polylactic acid (PLA). Nanofibers were characterized by Scanning Electron Microscopy (SEM) and Thermogravimetric Analysis (TGA). According to the SEM results, it is seen that the essential oil is composited with prominent spheroidal structures in PLA nanofiber structure, and nanofiber diameter obtained is approximately 76.8 nm. Its decomposition temperature is about 320°C. Nanofibers obtained from tangerine peels and their antibacterial properties, can be recommended use for food preservation and medicine fields.
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