{"title":"碘酸铅晶体的XRD, UV-VIS, PL和热研究","authors":"Amit B. Patil, Sandip K. Nerkar","doi":"10.14445/23948884/ijmse-v9i2p103","DOIUrl":null,"url":null,"abstract":"The lead iodate crystals have been grown in sodium meta-silicate gel using the single diffusion method at room temperature. The grown crystals were characterized by X-ray powder diffraction (XRD), UV, PL, and TGA/DSC. The crystal system is confirmed to be orthorhombic, having lattice parameters a= 16.70Å, b= 5.578Å and c= 6.083Å by powder X-ray diffraction analysis. The crystal's optical properties were characterized using UV-visible and Photoluminescence (PL) spectroscopy. TGA and DTA/DSC analysis show remarkable thermal stability.","PeriodicalId":481230,"journal":{"name":"SSRG international journal of materials science and engineering","volume":"17 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-08-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"XRD, UV-VIS, PL and Thermal Studies of Lead Iodate Crystals\",\"authors\":\"Amit B. Patil, Sandip K. Nerkar\",\"doi\":\"10.14445/23948884/ijmse-v9i2p103\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The lead iodate crystals have been grown in sodium meta-silicate gel using the single diffusion method at room temperature. The grown crystals were characterized by X-ray powder diffraction (XRD), UV, PL, and TGA/DSC. The crystal system is confirmed to be orthorhombic, having lattice parameters a= 16.70Å, b= 5.578Å and c= 6.083Å by powder X-ray diffraction analysis. The crystal's optical properties were characterized using UV-visible and Photoluminescence (PL) spectroscopy. TGA and DTA/DSC analysis show remarkable thermal stability.\",\"PeriodicalId\":481230,\"journal\":{\"name\":\"SSRG international journal of materials science and engineering\",\"volume\":\"17 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-08-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"SSRG international journal of materials science and engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.14445/23948884/ijmse-v9i2p103\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"SSRG international journal of materials science and engineering","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.14445/23948884/ijmse-v9i2p103","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
XRD, UV-VIS, PL and Thermal Studies of Lead Iodate Crystals
The lead iodate crystals have been grown in sodium meta-silicate gel using the single diffusion method at room temperature. The grown crystals were characterized by X-ray powder diffraction (XRD), UV, PL, and TGA/DSC. The crystal system is confirmed to be orthorhombic, having lattice parameters a= 16.70Å, b= 5.578Å and c= 6.083Å by powder X-ray diffraction analysis. The crystal's optical properties were characterized using UV-visible and Photoluminescence (PL) spectroscopy. TGA and DTA/DSC analysis show remarkable thermal stability.
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