Ruihao Zhang, Bing Wang, Zhanqiang Liu, Qinghua Song
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引用次数: 0
摘要
单晶硅由于原子间晶格结构不对称、不均匀而具有各向异性,影响了单晶硅的变形和断裂性能。本文旨在研究晶体取向对单晶硅高速刮擦过程中材料变形和去除行为的影响。研制了一种高速刻划装置,最高刻划速度可达40 m/s。在1 m/s ~ 30 m/s的速度范围内,对(001)、(110)和(111)晶面进行了倾斜划痕实验。随着刻划深度的增加,分析了硅在不同晶体取向上的韧脆转变。实验结果表明,沿“[”¯(“1”)”方向的抓痕(111)平面上的“10]”呈现出最大的韧脆过渡临界残余深度。在刮擦过程中,硅的韧性变形主要由Si-I相转变为Si-IV相和a-Si相,而在“[”¯(“1”)”范围内的刮擦试验(111)面上“10]”方向的材料非晶化程度最大。该研究可为优化不同晶向单晶硅元件的工艺参数提供指导。
EFFECT OF CRYSTALLOGRAPHIC ORIENTATION ON MATERIAL REMOVAL BEHAVIOR DURING HIGH SPEED SCRATCHING OF MONOCRYSTALLINE SILICON
Monocrystalline silicon has anisotropic attributes due to asymmetric and non-uniform interatomic lattice structures, which affects its deformation and fracture properties. This paper aims to investigate the effect of crystallographic orientation on the material deformation and removal behavior during high speed scratching of monocrystalline silicon. A high-speed scratching setup is developed which can achieve the highest scratching speed of 40 m/s. Inclined scratching experiments are conducted on (001), (110) and (111) crystallographic planes over the speed range of 1 m/s to 30 m/s. As the scratching depth increases, the ductile-to-brittle transition of silicon at different crystallographic orientations are analyzed. The experimental results suggest that scratching in the direction of "[" ¯("1" ) "10]" on (111) plane presents the largest critical residual depth of ductile-to-brittle transition. Phase transformation from Si-I to the phases of Si-IV and a-Si dominates ductile deformation of silicon during scratching process, while scratching tests in "[" ¯("1" ) "10]" direction on (111) plane demonstrates the largest degree of material amorphization. This study can provide guidance for optimizing processing parameters of monocrystalline silicon components with different crystallographic orientations.