脉冲激光烧蚀不同介质制备铜纳米颗粒及其物理性质研究

Awatif Sabir Jasim, Awrad Subhi Mahmood
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引用次数: 0

摘要

本研究采用脉冲激光烧蚀的方法制备了铜纳米颗粒(CuNPs),研究是在多个脉冲(700p/s)改变液体介质(乙醇、去离子水、蒸馏水)的作用下,使用(调q Nd-YAG)激光器进行的。在532nm波长和100mJ能量下,在乙醇、蒸馏水和去离子水介质中制备的样品的结果显示,CuNPs的平均半径分别为58.3、61.6和46.1 nm,呈球形。铜在(3250 ~ 3550)处的光谱主要是由于(O-H)透明羟基的膨胀和在三种溶剂(乙醇、去离子水、蒸馏水)的条件下发生的。XRD结果表明,在去离子水、蒸馏水和乙醇中制备的CuO纳米颗粒无杂质,结晶高度高,晶粒尺寸分别为2 θ(20.094、19.949、38.045)nm。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Preparation of Copper Nanoparticles Using Different Media by Pulsed Laser Ablation and Study of Their Physical Properties
In this study, copper nanoparticles (CuNPs) were prepared using the pulsed laser ablation method, and the study was conducted under the effect of changing the liquid medium (ethanol, deionized water, distilled water) with a number of pulses (700p/s) and using a (Q-switched Nd-YAG) laser. At a wavelength of 532nm and an energy of 100mJ, the results of the samples prepared in a medium (ethanol, distilled water, deionized water) showed the average radii of CuNPs (58.3, 61.6, 46.1 nm, respectively) with a spherical shape. The spectrum of copper at (3250 to 3550 ) is mainly due to the expansion of (O-H) the clear hydroxyl group and under the conditions of the three solvents (ethanol, deionized water, distilled water). The XRD results showed that the CuO nanoparticles are free of impurities and crystallized High and the crystallite size was calculated at 2theta (20.094, 19.949, 38.045) nm for the samples in (deionized water, distilled water, and ethanol), respectively.
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