{"title":"电纺丝法生产 PAN 基纳米纤维过程变量的统计建模","authors":"Ebubekir Sıddık AYDIN, İbrahim KORKUT","doi":"10.2339/politeknik.1247175","DOIUrl":null,"url":null,"abstract":"In this study, the effects of the electrospinning operating parameters such as flow rate (1-5 ml/h), voltage (15-30 kV), and distance to the collector (100-200 mm) on the physical properties of PAN-based nanofibers were investigated statistically by applying the central composite design method. The minimum nanofiber diameter was found to be 366.5 nm, under operating conditions of 5 ml/h flow rate, 30 kV, and 100 mm distance to the collector. Experimental conditions of 15 kV, 5 ml/h flow rate, and a 200 mm distance to the collector, a maximum porosity value of 0.446 was obtained. Similarly to the porosity, the water absorption capacity (WAC) value did not show a linear increase, and the maximum absorption capacity was calculated as 5712%, and at that point where the diameter is relatively large and the porosity is low.","PeriodicalId":44937,"journal":{"name":"Journal of Polytechnic-Politeknik Dergisi","volume":"70 1","pages":"0"},"PeriodicalIF":0.4000,"publicationDate":"2023-04-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"PAN Bazlı Nanofiberlerin Elektroeğirme ile Üretiminde Proses Değişkenlerinin İstatistiksel Modellenmesi\",\"authors\":\"Ebubekir Sıddık AYDIN, İbrahim KORKUT\",\"doi\":\"10.2339/politeknik.1247175\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this study, the effects of the electrospinning operating parameters such as flow rate (1-5 ml/h), voltage (15-30 kV), and distance to the collector (100-200 mm) on the physical properties of PAN-based nanofibers were investigated statistically by applying the central composite design method. The minimum nanofiber diameter was found to be 366.5 nm, under operating conditions of 5 ml/h flow rate, 30 kV, and 100 mm distance to the collector. Experimental conditions of 15 kV, 5 ml/h flow rate, and a 200 mm distance to the collector, a maximum porosity value of 0.446 was obtained. Similarly to the porosity, the water absorption capacity (WAC) value did not show a linear increase, and the maximum absorption capacity was calculated as 5712%, and at that point where the diameter is relatively large and the porosity is low.\",\"PeriodicalId\":44937,\"journal\":{\"name\":\"Journal of Polytechnic-Politeknik Dergisi\",\"volume\":\"70 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.4000,\"publicationDate\":\"2023-04-02\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Polytechnic-Politeknik Dergisi\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2339/politeknik.1247175\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"ENGINEERING, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Polytechnic-Politeknik Dergisi","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2339/politeknik.1247175","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"ENGINEERING, MULTIDISCIPLINARY","Score":null,"Total":0}
PAN Bazlı Nanofiberlerin Elektroeğirme ile Üretiminde Proses Değişkenlerinin İstatistiksel Modellenmesi
In this study, the effects of the electrospinning operating parameters such as flow rate (1-5 ml/h), voltage (15-30 kV), and distance to the collector (100-200 mm) on the physical properties of PAN-based nanofibers were investigated statistically by applying the central composite design method. The minimum nanofiber diameter was found to be 366.5 nm, under operating conditions of 5 ml/h flow rate, 30 kV, and 100 mm distance to the collector. Experimental conditions of 15 kV, 5 ml/h flow rate, and a 200 mm distance to the collector, a maximum porosity value of 0.446 was obtained. Similarly to the porosity, the water absorption capacity (WAC) value did not show a linear increase, and the maximum absorption capacity was calculated as 5712%, and at that point where the diameter is relatively large and the porosity is low.