{"title":"研究锰掺杂对硫化锌结构、形貌和光学性能的影响","authors":"","doi":"10.56042/ijpap.v61i9.3490","DOIUrl":null,"url":null,"abstract":"By utilising hydrothermal approach undoped and Mn-doped ZnS was synthesized and characterized by using X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDX), Field emission scanning electron microscopy (FE-SEM), Fourier transform infrared spectroscopy (FT-IR) and UV-Visible spectroscopy. The XRD pattern confirmed the cubic sphalerite crystal structure of prepared nanoparticles. Due to Mn doping, size of crystallite for all the samples was increased. FE-SEM images showed spherical morphology of synthesized samples. The EDX spectrum confirms the presence of Mn in the doped sample. FTIR spectrum showed that doping shifts the position of Zn-S absorption band. A red shift was observed in the absorption maxima and the bandgap was decreased with increasing doping percentage from 0 to 10%.","PeriodicalId":0,"journal":{"name":"","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"To Study the Impact of Mn Doping on Structural, Morphological and Optical Properties of Zinc Sulfide\",\"authors\":\"\",\"doi\":\"10.56042/ijpap.v61i9.3490\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"By utilising hydrothermal approach undoped and Mn-doped ZnS was synthesized and characterized by using X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDX), Field emission scanning electron microscopy (FE-SEM), Fourier transform infrared spectroscopy (FT-IR) and UV-Visible spectroscopy. The XRD pattern confirmed the cubic sphalerite crystal structure of prepared nanoparticles. Due to Mn doping, size of crystallite for all the samples was increased. FE-SEM images showed spherical morphology of synthesized samples. The EDX spectrum confirms the presence of Mn in the doped sample. FTIR spectrum showed that doping shifts the position of Zn-S absorption band. A red shift was observed in the absorption maxima and the bandgap was decreased with increasing doping percentage from 0 to 10%.\",\"PeriodicalId\":0,\"journal\":{\"name\":\"\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0,\"publicationDate\":\"2023-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.56042/ijpap.v61i9.3490\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.56042/ijpap.v61i9.3490","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
To Study the Impact of Mn Doping on Structural, Morphological and Optical Properties of Zinc Sulfide
By utilising hydrothermal approach undoped and Mn-doped ZnS was synthesized and characterized by using X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDX), Field emission scanning electron microscopy (FE-SEM), Fourier transform infrared spectroscopy (FT-IR) and UV-Visible spectroscopy. The XRD pattern confirmed the cubic sphalerite crystal structure of prepared nanoparticles. Due to Mn doping, size of crystallite for all the samples was increased. FE-SEM images showed spherical morphology of synthesized samples. The EDX spectrum confirms the presence of Mn in the doped sample. FTIR spectrum showed that doping shifts the position of Zn-S absorption band. A red shift was observed in the absorption maxima and the bandgap was decreased with increasing doping percentage from 0 to 10%.
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