测试中二甲胺中磷酸化苯胺的最佳脱氨状态。

Hainunnisa Syafitriza, Budhi Oktavia, Hary Sanjaya, Hardeli Hardeli
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引用次数: 0

摘要

介孔二氧化硅是具有2- 50nm孔径的固体二氧化硅。对二氧化硅进行改性是为了提高二氧化硅对阴离子的吸附能力,其中一种阴离子是磷酸阴离子。所使用的改性化合物是二甲胺。二氧化硅和二甲胺可以通过添加一种连接化合物即GPTMS结合。将改性后的二氧化硅用于吸附磷酸阴离子,观察二氧化硅对磷酸阴离子的吸附效果。二氧化硅吸附磷酸盐离子的吸附量为0.0172 mg/g,吸附率为88.09%。盐酸解吸得到的解吸磷酸盐浓度为0.773 mg/L,解吸率为89.02%;硫酸解吸得到的解吸磷酸盐浓度为0.437 mg/L,解吸率为48.81%。盐酸浓度变化为0.010 M、0.025 M、0.050 M、0.075 M、0.10 M、0.15 M和0.20 M, 0.1 M浓度下最大解吸量为0.0086 mg,解吸率为100%。
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Uji Kondisi Optimum Desorpsi Anion Fosfat pada Silika Mesopori Termodifikasi DMA (Dimethylamine)
Mesoporous silica is solid silica having a pore size of 2-50 nm. Silica modification is done to increase the ability of silica to absorb anions, one of which is phosphate anion. The modifier compound used is dimethylamine. Silica and dimethylamine can bind with the addition of a linking compound, namely GPTMS. This modified silica can be used to adsorb phosphate anions to see the absorption of silica against phosphate anions. Phosphate ion adsorption using silica has an adsorption capacity of 0.0172 mg/g with an absorption percentage of 88.09%. Desorption with hydrochloric acid obtained a desorbed phosphate concentration of 0.773 mg/L with a desorption percentage of 89.02% while using sulfuric acid the desorbed phosphate concentration was 0.437 mg/L with a desorption percentage of 48.81%. The concentration variations of hydrochloric acid were 0.010 M, 0.025 M, 0.050 M, 0.075 M, 0.10 M, 0.15 M and 0.20 M. The maximum desorption result at 0.1 M concentration was 0.0086 mg with a percentage of 100%.
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