树脂离子交换法提取广藿香油中的铁离子

A. Jaenuri, Thafie Ghilas Anarchie, K. Sumada
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摘要

广藿香是印尼精油出口中最大的非石油出口商品。然而,印尼广藿香油的质量被认为非常低。传统的广藿香油蒸馏是在小容量中进行的,采用基于沸点或其中一种挥发性成分差异较大的简单蒸馏方法。该工艺生产的广藿香油酸值大于8,油色偏黑,醇度小于30%,含水量高,质量差。广藿香油中含有大量的铁金属证明了这一点。所生产的广藿香油中含有大量的铁,因此需要进一步加工以降低广藿香油中的铁含量。利用树脂作为金属铁吸附剂是降低金属铁含量的一种方法。分别将50克、150克和250克的树脂加入200毫升广藿香油中。然后以200 rpm的搅拌速度进行搅拌过程,搅拌时间分别为30、60和90分钟。结果表明,当广藿香油中Fe含量为1.42 mg/Kg、接触时间为90 min、树脂用量为250 g时,吸附效果最佳,去除率最高为87.5%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Fe ion extraction in patchouli oil with ion exchange using resin
Patchouli is the largest non-oil export commodity among essential oil exports in Indonesia. However, the quality of patchouli oil in Indonesia is considered to be very low. Traditional patchouli oil distillation is carried out in a small capacity and uses a simple distillation method based on a large difference in boiling points or one of the volatile components. This process produces poor quality patchouli oil such as acid number more than 8, dark oil, patchouli alcohol less than 30%, and high water content. This is evidenced by the large amount of Fe metal contained in patchouli oil. Patchouli oil produced contains a lot of iron in its yield, so it needs further processing to reduce the Fe content in patchouli oil. The use of resin as an adsorbent for Fe metal is one way to reduce the Fe metal content. Resin weighing 50, 150 and 250 grams was added to 200 ml of patchouli oil. Then the stirring process was carried out with a stirring speed of 200 rpm with time variations of 30, 60 and 90 minutes. The results obtained showed the best adsorption process with Fe content in patchouli oil of 1.42 mg/Kg, contact time of 90 minutes and amount of resin of 250 grams with the largest percentage of removal of 87.5%.
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