添加氢氧化钾(KOH)活化剂的椰子纤维合成导电碳片

Dian Surya Sinaga, N. Indayaningsih
{"title":"添加氢氧化钾(KOH)活化剂的椰子纤维合成导电碳片","authors":"Dian Surya Sinaga, N. Indayaningsih","doi":"10.32734/jotp.v4i1.8177","DOIUrl":null,"url":null,"abstract":"Research has been carried out on manufacturing conductive carbon sheets using carbon as raw material from coconut fiber with a Potassium Hydroxide (KOH) activator. First, activation was carried out using 1000 ml of 6M KOH solution mixed with 100 grams of carbon at 100℃ for 72 hours. Next, the carbon is pyrolyzed at temperatures of 900℃, 1100℃, and 1300℃ for 2 hours. Next, the pyrolysis carbon was washed with 2M HCl for 24 hours and washed with distilled water until the pH was neutral. Electrical resistance measurements were made with torque variations of 10, 20, and 30 kgf. cm using the four-point probe method, then the conductivity value was calculated. Finally, carbon characterization was carried out using the XRD tool. The increase in pyrolysis temperature causes the carbon conductivity to increase, which is 2.3855- 4.2340 S/cm at 900℃ and 6.8203-11.4577 S/cm at 1300℃. XRD analysis showed a sharp and narrow increase in diffraction peaks with each increase in pyrolysis temperature, indicating that carbon has a crystal structure close to graphite which is more ordered than carbon without an activator.","PeriodicalId":323487,"journal":{"name":"Journal of Technomaterial Physics","volume":"36 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2022-02-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis of Conductive Carbon Sheet From Coconut Fiber with the Addition of Potassium Hydroxide (KOH) Activator\",\"authors\":\"Dian Surya Sinaga, N. Indayaningsih\",\"doi\":\"10.32734/jotp.v4i1.8177\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Research has been carried out on manufacturing conductive carbon sheets using carbon as raw material from coconut fiber with a Potassium Hydroxide (KOH) activator. First, activation was carried out using 1000 ml of 6M KOH solution mixed with 100 grams of carbon at 100℃ for 72 hours. Next, the carbon is pyrolyzed at temperatures of 900℃, 1100℃, and 1300℃ for 2 hours. Next, the pyrolysis carbon was washed with 2M HCl for 24 hours and washed with distilled water until the pH was neutral. Electrical resistance measurements were made with torque variations of 10, 20, and 30 kgf. cm using the four-point probe method, then the conductivity value was calculated. Finally, carbon characterization was carried out using the XRD tool. The increase in pyrolysis temperature causes the carbon conductivity to increase, which is 2.3855- 4.2340 S/cm at 900℃ and 6.8203-11.4577 S/cm at 1300℃. XRD analysis showed a sharp and narrow increase in diffraction peaks with each increase in pyrolysis temperature, indicating that carbon has a crystal structure close to graphite which is more ordered than carbon without an activator.\",\"PeriodicalId\":323487,\"journal\":{\"name\":\"Journal of Technomaterial Physics\",\"volume\":\"36 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-02-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Technomaterial Physics\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.32734/jotp.v4i1.8177\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Technomaterial Physics","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.32734/jotp.v4i1.8177","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

以椰子纤维为原料,用氢氧化钾(KOH)活化剂制备导电碳片进行了研究。首先,用1000ml的6M KOH溶液与100g碳混合,在100℃下活化72小时。接下来,碳在900℃,1100℃和1300℃的温度下热解2小时。然后将热解炭用2M HCl洗涤24小时,再用蒸馏水洗涤至pH为中性。电阻测量是在10、20和30 kgf的扭矩变化下进行的。采用四点探针法,计算电导率值。最后,利用XRD工具进行碳的表征。随着热解温度的升高,碳的电导率增大,900℃时为2.3855 ~ 4.2340 S/cm, 1300℃时为6.8203 ~ 11.4577 S/cm。XRD分析表明,随着热解温度的升高,碳的衍射峰呈明显的窄增长,表明碳的晶体结构接近石墨,比未添加活化剂的碳更有序。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis of Conductive Carbon Sheet From Coconut Fiber with the Addition of Potassium Hydroxide (KOH) Activator
Research has been carried out on manufacturing conductive carbon sheets using carbon as raw material from coconut fiber with a Potassium Hydroxide (KOH) activator. First, activation was carried out using 1000 ml of 6M KOH solution mixed with 100 grams of carbon at 100℃ for 72 hours. Next, the carbon is pyrolyzed at temperatures of 900℃, 1100℃, and 1300℃ for 2 hours. Next, the pyrolysis carbon was washed with 2M HCl for 24 hours and washed with distilled water until the pH was neutral. Electrical resistance measurements were made with torque variations of 10, 20, and 30 kgf. cm using the four-point probe method, then the conductivity value was calculated. Finally, carbon characterization was carried out using the XRD tool. The increase in pyrolysis temperature causes the carbon conductivity to increase, which is 2.3855- 4.2340 S/cm at 900℃ and 6.8203-11.4577 S/cm at 1300℃. XRD analysis showed a sharp and narrow increase in diffraction peaks with each increase in pyrolysis temperature, indicating that carbon has a crystal structure close to graphite which is more ordered than carbon without an activator.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信