真空选择性激光熔化制备钛合金板的实验研究

SPIE LASE Pub Date : 2016-04-06 DOI:10.1117/12.2212654
Yuji Sato, M. Tsukamoto, Y. Yamashita, S. Masuno, N. Abe
{"title":"真空选择性激光熔化制备钛合金板的实验研究","authors":"Yuji Sato, M. Tsukamoto, Y. Yamashita, S. Masuno, N. Abe","doi":"10.1117/12.2212654","DOIUrl":null,"url":null,"abstract":"We demonstrated that a Ti-6Al-4V plate, which is clinically used for artificial bone and hard tissue implant in human body because of their light and biocompatibility, were fabricated by SLM process in vacuum. The chamber’s pressure was set to 1.0×10-3 Pa to prevent the Ti64 powder from oxidizing. The base plate of the powder bed was vertically dropped in determined steps, and Ti64 powder supplied from the powder feeder was then smoothed by a roller on top of the powder bed. The single-mode fiber laser irradiated and melted the powder bed to make a molten pool in order to form 2D metallic structures In order to investigate the laser melting and solidification dynamics, a process of Ti 64 plate fabrication was captured by high speed video camera. It was also determined that crystal orientation was evaluated with X-ray diffraction (XRD) and energy dispersive X-ray (EDX) spectroscopy From EDX analysis, the chemical compounds were not changed from powder to fabricated sample. And it was recorded from the powder peaks of α (1011), α (0002), α (1010), and α (1012) that the crystal orientation is composed mainly of martensitic alpha by XRD analysis. Diffraction peaks corresponding to β (110) were detected in vacuum SLM processed samples.","PeriodicalId":314691,"journal":{"name":"SPIE LASE","volume":"60 2 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2016-04-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Experimental study on Ti alloy plate fabrication by vacuum selective laser melting\",\"authors\":\"Yuji Sato, M. Tsukamoto, Y. Yamashita, S. Masuno, N. Abe\",\"doi\":\"10.1117/12.2212654\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"We demonstrated that a Ti-6Al-4V plate, which is clinically used for artificial bone and hard tissue implant in human body because of their light and biocompatibility, were fabricated by SLM process in vacuum. The chamber’s pressure was set to 1.0×10-3 Pa to prevent the Ti64 powder from oxidizing. The base plate of the powder bed was vertically dropped in determined steps, and Ti64 powder supplied from the powder feeder was then smoothed by a roller on top of the powder bed. The single-mode fiber laser irradiated and melted the powder bed to make a molten pool in order to form 2D metallic structures In order to investigate the laser melting and solidification dynamics, a process of Ti 64 plate fabrication was captured by high speed video camera. It was also determined that crystal orientation was evaluated with X-ray diffraction (XRD) and energy dispersive X-ray (EDX) spectroscopy From EDX analysis, the chemical compounds were not changed from powder to fabricated sample. And it was recorded from the powder peaks of α (1011), α (0002), α (1010), and α (1012) that the crystal orientation is composed mainly of martensitic alpha by XRD analysis. Diffraction peaks corresponding to β (110) were detected in vacuum SLM processed samples.\",\"PeriodicalId\":314691,\"journal\":{\"name\":\"SPIE LASE\",\"volume\":\"60 2 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2016-04-06\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"SPIE LASE\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1117/12.2212654\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"SPIE LASE","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1117/12.2212654","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1

摘要

采用真空SLM工艺制备了Ti-6Al-4V板,该板具有轻质、生物相容性好等优点,可用于人体人工骨和硬组织植入。为了防止Ti64粉末氧化,将腔室的压力设置为1.0×10-3 Pa。将粉床底板按确定的步骤垂直下落,然后由给粉机供应的Ti64粉末通过粉床顶部的滚轮进行平滑。采用单模光纤激光对粉末层进行辐照熔化形成熔池,形成二维金属结构。为了研究激光熔化和凝固动力学,采用高速摄像机捕捉了Ti 64板的制备过程。用x射线衍射(XRD)和能量色散x射线(EDX)光谱分析了晶体取向。从EDX分析来看,从粉末到制备样品的化学成分没有变化。粉末α(1011)、α(0002)、α(1010)和α(1012)峰的XRD分析表明,晶体取向主要由马氏体α组成。在真空SLM处理的样品中检测到β(110)衍射峰。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Experimental study on Ti alloy plate fabrication by vacuum selective laser melting
We demonstrated that a Ti-6Al-4V plate, which is clinically used for artificial bone and hard tissue implant in human body because of their light and biocompatibility, were fabricated by SLM process in vacuum. The chamber’s pressure was set to 1.0×10-3 Pa to prevent the Ti64 powder from oxidizing. The base plate of the powder bed was vertically dropped in determined steps, and Ti64 powder supplied from the powder feeder was then smoothed by a roller on top of the powder bed. The single-mode fiber laser irradiated and melted the powder bed to make a molten pool in order to form 2D metallic structures In order to investigate the laser melting and solidification dynamics, a process of Ti 64 plate fabrication was captured by high speed video camera. It was also determined that crystal orientation was evaluated with X-ray diffraction (XRD) and energy dispersive X-ray (EDX) spectroscopy From EDX analysis, the chemical compounds were not changed from powder to fabricated sample. And it was recorded from the powder peaks of α (1011), α (0002), α (1010), and α (1012) that the crystal orientation is composed mainly of martensitic alpha by XRD analysis. Diffraction peaks corresponding to β (110) were detected in vacuum SLM processed samples.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信