Kerim Emre Öksüz
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摘要

采用高能球磨工艺,用不同尺寸的氧化铝(Al2O3)颗粒进行机械合金化,制备了具有增强Cu基的铜(Cu)复合材料。初始材料由惰性气体雾化球形电解铜粉末组成,其中含有0.5 wt. %的商用Al2O3粉末,粒径范围为10µm至1µm。对不同Al2O3粒度的Cu粉末进行500转/分的高能球磨3小时,以获得Al2O3在Cu基体中的均匀分布。将高能球磨后的粉末在500 MPa下进行冷压,在880℃氩气中等温烧结1.5小时。采用x射线衍射分析(XRD)、场发射扫描电镜(FE-SEM)、能量色散x射线能谱(EDXS)、密度和宏观硬度测试对制备的铜复合材料进行了表征。通过摩擦针盘式实验研究了Cu基体的磨损性能和机理,结果表明,与粗Al2O3颗粒相比,细分散Al2O3颗粒结合到Cu基体中的增强效果更显著。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
YÜKSEK ENERJİLİ ÖĞÜTME İLE ÜRETİLEN Al2O3 TAKVİYELİ CU KOMPOZİTLERDE PARÇACIK BOYUTUNUN ETKİSİ
Production of copper (Cu) composites with a reinforced Cu matrix using mechanical alloying with Aluminum oxide (Al2O3) particles of different sizes was achieved using high-energy ball milling procedure. The initial materials consisted of inert gas-atomized spherical electrolytic Cu powders containing 0.5 wt. % commercial Al2O3 powders, with particle sizes ranging from 10 µm to 1 µm. Cu powders with different particle sizes of Al2O3 were high-energy ball milled at 500 rpm for 3 hours to attain a consistent distribution of Al2O3 throughout in the Cu matrix. The powders that were high-energy ball milled were then subjected to cold-pressing at 500 MPa and isothermally sintered for 1.5 hours at 880°C in an Ar atmosphere. The fabricated copper composite materials were characterized using X-ray diffraction analysis (XRD), field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDXS), density and macrohardness tests. The wear properties and mechanism were investigated through tribological pin-on-disc experiments, which revealed that the reinforcing effect was more significant when finely dispersed Al2O3 particles were combined into the Cu matrix compared to coarse Al2O3 particles.
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