用氢氧化钙与纳米氢氧化钙对考古描纸脱酸的比较研究

Amany Krorra, W. Wahba, Marwa Abu Elleif
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引用次数: 0

摘要

本研究旨在进行实验研究,比较使用描图纸的脱酸效果;溶解在乙醇中的氢氧化钙;与使用溶解在异丙醇中的纳米氢氧化钙相比。然后;进行测试和分析,比较两种材料,以便选择最合适的一种材料,用于埃及“埃及地理学会”的考古追踪地图。对示踪纸样品进行加速老化后的处理方法进行了评估,以研究脱酸材料的效率,使用FTIR分析(傅里叶变换红外光谱)通过比较处理样品和标准样品中纤维素、半纤维素和木质素的特征官能团的吸收光谱的强度和区域来识别其官能团的化学变化。也;镜检;采用数码光学显微镜、扫描电子显微镜(SEM);检查处理过的纸张样品的表面外观。此外;通过使用色度计来评估处理过的纸张样品在老化前和老化前发生的颜色变化。通过测定纸样的拉伸强度和伸长率来评价纸样的力学性能。此外;通过测量处理后样品与标准样品的pH值来评价脱酸的质量。纳米氢氧化钙处理对纸张的化学成分有轻微的影响,并改善了脱酸效果;和氢氧化钙相比。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
COMPARATIVE STUDY USING CALCIUM HYDROXIDE AND NANO CALCIUM HYDROXIDE TO DEACIDIFICATION OF ARCHAEOLOGICAL TRACING PAPER
The research aims to conduct an experimental study to compare the effect of the Deacidification of tracing paper using; Calcium Hydroxide dissolved in Ethyl alcohol; in comparison with that use Nanocalcium Hydroxide dissolved in Isopropyl alcohol. Then; performing tests and analysis to compare between the two materials, in order to select the most suitable one to deacidify archaeological tracing maps at the “Egyptian Geographical Society” in, Egypt. The treatment methods used on tracing paper samples have been assessed after accelerated aging procedures, to study the efficiency of the Deacidification materials, using FTIR analysis (Fourier transform infrared spectroscopy) to identify the chemical changes in the functional groups of cellulose, hemicelluloses and lignin, by comparing the intensity and regions of the absorption spectrum of their characteristic functional groups, in both the treated and standard samples. Also; microscopic examination was conducted; using Digital Light Microscope, and the Scanning Electron Microscope (SEM); to examine the surface appearance of the treated paper sample. Moreover; the visual properties by using a colorimeter to assess the colour changes that occurred in the treated paper samples before and aging. The mechanical properties of the paper samples were evaluated by measuring the tensile strength and elongation percentage. Furthermore; the quality of the Deacidification was evaluated by measuring the pH of the treated samples in comparison with the standard samples. The Nanocalcium Hydroxide treatment was proved to have a slight effect on the chemical composition of the paper and an improved Deacidification; in comparison to Calcium Hydroxide.
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