复合石墨粉体的电化学制备方法

R. K. Salakhova, A. B. Tikhoobrazov, A. S. Yaroshenko, T. Smirnova
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引用次数: 0

摘要

提出了在石墨粉级GL-1上沉积镍、铜和Cu-Ni涂层制备复合石墨粉的电化学方法,保证了复合粉末材料的生产。设计了一种装置和工艺方案,提出了石墨电化学金属化的循环方法,使制备具有一定化学成分的复合石墨粉末成为可能。提出了在石墨粉级GL-1上沉积镍、铜和Cu-Ni涂层制备复合石墨粉的电化学方法,保证了复合粉末材料的生产。设计了一种装置和工艺方案,提出了石墨电化学金属化的循环方法,使制备具有一定化学成分的复合石墨粉末成为可能。对石墨粉镀镍工艺进行了优化,得到了回归方程,并给出了回归系数的离散分析结果,表明所建立的回归模型充分性和统计学意义。用光学显微镜测定了镍、铜和铜镍复合镀层的厚度。结果表明,石墨粉末金属化的电解方法使沉积连续涂层成为可能,每个石墨颗粒形成一个壳(胶囊)。介绍了镀镍石墨粉的理化性质(堆积密度、流动性、粒度和化学成分)的研究结果。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Electrochemical method for obtaining of composite graphite powder
An electrochemical method for producing a composite graphite powder by depositing nickel, copper and Cu—Ni coatings on graphite powder grade GL-1 is proposed, which ensures the production of a clad powder material. An installation, a technological scheme was developed, and a cyclic method of electrochemical metallization of graphite was proposed, which makes it possible to obtain a composite graphite powder of a given chemical composition. An electrochemical method for producing a composite graphite powder by depositing nickel, copper and Cu-Ni coatings on graphite powder grade GL-1 is proposed, which ensures the production of a clad powder material. An installation, a technological scheme was developed, and a cyclic method of electrochemical metallization of graphite was proposed, which makes it possible to obtain a composite graphite powder of a given chemical composition. The graphite powder nickel plating process was optimized, a regression equation was obtained, and the results of the dispersion analysis of regression coefficients were presented, indicating the adequacy and statistical significance of the obtained regression model. The thickness of nickel, copper and combined Cu-Ni coatings was determined by optical microscopy. It is shown that the electrolytic method of graphite powder metallization makes it possible to deposit continuous coatings with the formation of a shell (capsule) for each graphite particle. Presents the results of a study of the physicochemical properties of nickel-plated graphite powder (bulk density, fluidity, granulometric and chemical composition).
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