电化学阳极氧化法制备阳极氧化二氧化钛纳米管薄膜的结构特性

N. Azhar, S. S. Shariffudin, R. A. Rani, S. Munirah, S. Nagaoka, M. Rusop
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引用次数: 0

摘要

发光二极管(LED)是利用半导体材料将电能转换为光能的固态照明。二氧化钛(TiO2)因其纯度高且易于在薄膜上合成而被广泛用于光电器件。采用电化学阳极氧化法制备了TiO2纳米管。对TiO2纳米管进行了无定形和450℃退火处理。450℃退火后的样品表面形貌均匀,顶层TiO2呈规则多孔结构。拉曼图显示,阳极氧化过程中TiO2样品由无定形向晶态转变。光学性质表明,450℃退火后的TiO2纳米管没有明显的吸光度边缘,这与纳米管材料缺氧有关。经450℃退火的TiO2纳米管薄膜具有应用于LED器件的潜力。发光二极管(LED)是利用半导体材料将电能转换为光能的固态照明。二氧化钛(TiO2)因其纯度高且易于在薄膜上合成而被广泛用于光电器件。采用电化学阳极氧化法制备了TiO2纳米管。对TiO2纳米管进行了无定形和450℃退火处理。450℃退火后的样品表面形貌均匀,顶层TiO2呈规则多孔结构。拉曼图显示,阳极氧化过程中TiO2样品由无定形向晶态转变。光学性质表明,450℃退火后的TiO2纳米管没有明显的吸光度边缘,这与纳米管材料缺氧有关。经450℃退火的TiO2纳米管薄膜具有应用于LED器件的潜力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Structural properties of anodic titanium dioxide (TiO2) nanotubes film via electrochemical anodization
Light emitting diode (LED) is solid state lighting uses semiconductor material and convert the electrical energy to light energy. Titanium dioxide (TiO2) was used in optoelectronic devices because it is good purity and easily synthesizing onto thin film. TiO2 nanotubes was prepared by electrochemical anodization method at room temperature. The TiO2 nanotubes was investigated amorphous and annealed sample at 450°C. The surface morphology revealed that sample annealed at 450°C showed uniformity with a regular porous on top layer of TiO2. Raman pattern showed the amorphous-to-crystalline anodic TiO2 sample transition with anodization. Optical properties showed the TiO2 nanotubes annealed at 450°C has not sharp absorbance edge and it is relates to the oxygen deficiency in nanotube material. The TiO2 nanotubes film annealed at 450°C has potential apply to LED devices.Light emitting diode (LED) is solid state lighting uses semiconductor material and convert the electrical energy to light energy. Titanium dioxide (TiO2) was used in optoelectronic devices because it is good purity and easily synthesizing onto thin film. TiO2 nanotubes was prepared by electrochemical anodization method at room temperature. The TiO2 nanotubes was investigated amorphous and annealed sample at 450°C. The surface morphology revealed that sample annealed at 450°C showed uniformity with a regular porous on top layer of TiO2. Raman pattern showed the amorphous-to-crystalline anodic TiO2 sample transition with anodization. Optical properties showed the TiO2 nanotubes annealed at 450°C has not sharp absorbance edge and it is relates to the oxygen deficiency in nanotube material. The TiO2 nanotubes film annealed at 450°C has potential apply to LED devices.
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