基于高性能纳米片/还原氧化石墨烯(rGO)纳米片的乙炔气体检测

Zikai Jiang, Weigen Chen, Yujiang He, Hongtao Zhang, Zhixian Zhang, Junsheng Chen, K. Wu
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引用次数: 0

摘要

基于金属氧化物(MOs)材料的油浸式变压器故障诊断是电力系统中最有前途的研究方向之一。本文采用可控水热法制备了四种含量的WO3纳米片/还原氧化石墨烯纳米复合材料。利用x射线衍射(XRD)和透射电子显微镜(TEM)对制备的纳米复合材料的微观结构进行了研究,结果表明WO3广泛分布在还原氧化石墨烯薄片中。利用自旋镀膜技术将纳米复合材料覆盖在气体传感器上,研究了WO3纳米片/还原氧化石墨烯纳米复合材料对温度为$50\ ^{\circ} $至$400\ ^{\circ}C$的多浓度C2H2气体的敏感性。研究结果表明,1 wt%的传感材料具有较低的工作温度、优异的响应和恢复时间、良好的长时间稳定性和显著的可恢复性。基于异质结电子交换理论可以解释高性能WO3/rGO材料的潜在机理。本文的研究成果对电力变压器故障诊断具有一定的指导意义。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Deteciton of Acetylene Gas based on high Performance $\text{WO}_{3}$ Nanolamellae/Reduced Graphene Oxide (rGO) Nanosheets
Oil-immersed transformer faults diagnosis based on Metal oxides (MOs) materials is one of the most promising research trends in power system. In this paper, four contents of WO3 nanolamellae/ reduced graphene oxide nanocomposites were compounded via controlled hydrothermal method. X-ray diffraction (XRD) and transmission electron microscopy (TEM) were used to investigate the microstructure of prepared nanocomposites and indicated WO3 were widely distributed among rGO sheets. Spin -coating technique was utilized for nanocomposites coverage on gas sensor and the sensitivity of WO3 nanolamellae/ reduced graphene oxide nanocomposites towards multi-concentrations of C2H2 gases with temperature ranging from $50\ ^{\circ}\mathrm{C}$ to $400\ ^{\circ}C$ was studied. The research results exhibited that 1 wt% sensing materials demonstrated a lower working temperature, outstanding response and recovery time, excellent long-time stability and remarkable recoverability. The potential mechanism of high performance WO3/rGO materials could be explained based on heterojunction electron exchange theory. Research outcomes presented in this paper can be the guidance to power transformer faults diagnosis to some degree.
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