{"title":"钼酸铜纳米颗粒的生物合成与表征","authors":"P. Santhiyadevi, K. Buvaneswari","doi":"10.30799/JNST.120.18040403","DOIUrl":null,"url":null,"abstract":"In the present work CuMoO 4 and P/CuMoO 4 nanoparticles were synthesized by simple precipitation method. The synthesized molybdate nanoparticles were characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), scanning electron microscopy (SEM) and UV-visible diffuse reflectance spectroscopy (UV-vis DRS). XRD results show that the average crystalline size of CuMoO 4 and P/CuMoO 4 nanoparticles were found to be 62.9 nm and 59.7 nm respectively. SEM results showed that CuMoO 4 nanoparticles composed of sphere like structure and P/CuMoO 4 with agglomeration. Four absorption bands at 721, 828, 898 and 967 cm -1 were observed in FT-IR spectrum. The sharp adsorption peak at 270-350 nm was observed in UV–vis DRS technique. The antimicrobial activities of synthesized nanoparticles were observed against various pathogens.","PeriodicalId":187599,"journal":{"name":"Journal of Nanoscience and Technology","volume":"1 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2018-06-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"5","resultStr":"{\"title\":\"Bio-Synthesis and Characterization of Copper Molybdate Nanoparticles\",\"authors\":\"P. Santhiyadevi, K. Buvaneswari\",\"doi\":\"10.30799/JNST.120.18040403\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In the present work CuMoO 4 and P/CuMoO 4 nanoparticles were synthesized by simple precipitation method. The synthesized molybdate nanoparticles were characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), scanning electron microscopy (SEM) and UV-visible diffuse reflectance spectroscopy (UV-vis DRS). XRD results show that the average crystalline size of CuMoO 4 and P/CuMoO 4 nanoparticles were found to be 62.9 nm and 59.7 nm respectively. SEM results showed that CuMoO 4 nanoparticles composed of sphere like structure and P/CuMoO 4 with agglomeration. Four absorption bands at 721, 828, 898 and 967 cm -1 were observed in FT-IR spectrum. The sharp adsorption peak at 270-350 nm was observed in UV–vis DRS technique. The antimicrobial activities of synthesized nanoparticles were observed against various pathogens.\",\"PeriodicalId\":187599,\"journal\":{\"name\":\"Journal of Nanoscience and Technology\",\"volume\":\"1 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2018-06-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"5\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Nanoscience and Technology\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.30799/JNST.120.18040403\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Nanoscience and Technology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.30799/JNST.120.18040403","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Bio-Synthesis and Characterization of Copper Molybdate Nanoparticles
In the present work CuMoO 4 and P/CuMoO 4 nanoparticles were synthesized by simple precipitation method. The synthesized molybdate nanoparticles were characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), scanning electron microscopy (SEM) and UV-visible diffuse reflectance spectroscopy (UV-vis DRS). XRD results show that the average crystalline size of CuMoO 4 and P/CuMoO 4 nanoparticles were found to be 62.9 nm and 59.7 nm respectively. SEM results showed that CuMoO 4 nanoparticles composed of sphere like structure and P/CuMoO 4 with agglomeration. Four absorption bands at 721, 828, 898 and 967 cm -1 were observed in FT-IR spectrum. The sharp adsorption peak at 270-350 nm was observed in UV–vis DRS technique. The antimicrobial activities of synthesized nanoparticles were observed against various pathogens.