PM hip316l和316LN的特性、特点和发展概述

Martin Östlund, T. Berglund
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引用次数: 0

摘要

PM HIP 316L是一种合金,自最近ASME规范案例批准以来,对核应用的兴趣越来越大。多年来,收集和评估了全面的数据和对其性质和特征的理解,本文将对此进行总结。由于PM HIP技术的早期发展,已经观察到PM HIP合金通常表现出更高的屈服强度与传统的对应物相比,这一特点适用于316L。在本文中,通过使用Hall-Petch关系以及Picker - ing和Irvine的经验推导的奥氏体不锈钢成分和晶粒尺寸之间的关系来证明这一点。此外,还提出了一种产生PM HIP 316L比传统制造的316L屈服强度增加的机制。结果还表明,低氧含量本身并不能保证良好或提高机械性能,但为了获得良好的性能,还有其他类似或甚至更重要的特性。本文的结果包括从EBSD测量中得出的微观结构性能,以及在不同地点生产的几种粉末棒的PM HIP 316L在广泛的测试温度范围内的拉伸和冲击性能,这些粉末棒经过各种HIP和热处理程序处理。最后,给出了一些关于PM hip316l蠕变性能的研究结果。奥氏体不锈钢316L是最常用的不锈钢牌号之一,这种合金在不同产品形式下的性能和性能是众所周知的。通过气体化和热等静压进行粉末冶金制造是一种已知的制造技术,可以产生等向组织,高清洁度和经常改进的机械性能。根据最近ASME规范对PM HIP 316L的批准[1],这种合金在这种制造过程中的性能越来越受到关注[2-4]。本文将概述PM HIP 316L/316LN的性能,性能如何受到不同制造工艺参数的影响,并比较它们与传统制造的对应产品的区别。微观结构PM - HIP制造的一大好处是制造的部件的微观结构是均匀的,各向同性的,并且具有高清洁度。所有这些特点也适用于PM HIP 316L/316LN,并将其转化为优异的超声可检测性[4]。在清洁度方面,PM HIP 316L/316LN中绝大多数非金属夹杂物的粒径都在2.8 μm以下,主要由氧化物组成[2,3]。氧化物可以来自熔体,这些熔体后来被困在粉末颗粒中(大块氧化物),也可以来自表面氧化层和氧化物
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Overview of Properties, Features and Developments of PM HIP 316L and 316LN
PM HIP 316L is an alloy that is of increased intere st for nuclear applications since its recent ASME code case approval. Over the years, com prehensive data and understanding of the properties and features have been collected and evaluated which will be summarized in this article. Since the early developments of the P M HIP technology it has been observed that PM HIP alloys generally exhibit higher yield streng ths compared to their conventional counterparts, a feature that applies well for 316L. In this article this is demonstrated, both by using the Hall-Petch relationship as well as Picker ing ́s and Irvine ́s empirically derived relationship between composition and grain size for austenitic stainless steels. Furthermore, a mechanism generating the increased yield strength i n PM HIP 316L vs conventionally manufactured 316L will be proposed. Results also sh ow t at low oxygen contents itself is not a guarantee for good or increased performance in fo rm of mechanical properties, but that there are other features that is of similar or perhaps ev en higher importance in order to achieve good properties. The results of this article includ e microstructural properties derived from EBSD measurements as well as tensile and impact pro perties in a wide range of test temperatures of PM HIP 316L from several powder bat ches manufactured at different locations and processed with various HIP and heat t r ment procedures. Finally, some results regarding creep properties of PM HIP 316L is presen ted. Introduction Austenitic stainless steel 316L is one of the most c mmonly known and used stainless steel grades and the performance and properties of this a lloy in different product forms is well known. Powder Metallurgical manufacturing via Gas A tomization and Hot Isostatic Pressing is a manufacturing technology known to generate iso tropic microstructures, high cleanliness and often improved mechanical properties. In light of he recent ASME code case approval for PM HIP 316L [1], the properties of this alloy v ia this manufacturing process has become of increasing interest [2-4]. This article will giv e an overview of the properties of PM HIP 316L/316LN, how properties can be affected by varyi ng manufacturing process parameters and compare how they differ from the conventionally manufactured counterparts. Microstructure One of the large benefits with PM HIP manufacturing s that the microstructures of the manufactured components are homogeneous, isotropic and have high cleanliness. All these features apply also for PM HIP 316L/316LN and trans l tes into excellent ultrasonic inspectability [4]. Regarding cleanliness, the clea r majority of the non-metallic inclusions found in PM HIP 316L/316LN are well below 2.8 μm in size and are predominately constituted by oxides [2,3]. The oxides can origina te either from the melt which are later trapped within the powder particles (bulk oxides) o r fr m the surface oxide layer and oxide
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