混合铁钴氧化物纳米示踪剂的合成及其在液体饲料混合质量评价中的应用

REPORTS OF THE NAS RK Pub Date : 2023-03-30 DOI:10.32014/2023.2518-1483.201

©. S. Mendigaliyeva, I. Irgibaeva, N. Barashkov, T. V. Sakhno, A. A. Aldongarov, Mendigaliyeva Svetlana, Samiguliyena — L.N. Gumilyov, Irgibaeva Irina Smailovna, Viktorivna, Aldongarov Anuar Akylkhanovich, ©. С. Мендіғалиевa, И.С. Иргибаевa, Н.Н. Барашков, T.В. Сахно, A. A. Aлдонгаров, Л.Н. Гумилев атындағы Еуразия, Ұлттық Университеті, Қазақстан Астана, Мендіғалиева Светлана, Самигуллиевна — Л.Н. Гумилев, Еуразия Ұлттық, ©. С. Мендигалиевa, С. Иргибаевa

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引用次数: 0

摘要

．将氯化亚铁、氯化铁、氯化钴和氢氧化铵的水溶液混合，继续搅拌加热形成胶体含钴磁铁矿，制备出氧化铁(95%以上)和氧化锰(5%以下)的纳米颗粒。制备的纳米颗粒在油酸铵和油酸二甲胺盐等表面活性剂水溶液中形成稳定的纳米示踪剂悬浮液的可能性已经得到证实。采用纳米颗粒跟踪分析(NTA)方法测定了纳米示踪剂的粒径，该方法基于对含有两种表面活性剂的水介质中纳米颗粒的直接可视化和分析。它经常发现中等大小的纳米颗粒不超过90纳米。使用准备好的可能性

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SYNTHESIS AND APPLICATION OF NANOTRACERS BASED ON MIXED IRON–COBALT OXIDE FOR EVALUATION OF THE QUALITY OF MIXING IN LIQUID FEED

. Nanoparticles combining iron oxide (higher 95 %) and manganese oxide (below 5 %) have been prepared by mixing aqueous solutions of ferrous chloride, ferric chloride, cobalt chloride and ammonium hydroxide following by continued stirring and heating the forming colloidal Co-containing magnetite. The possibility of forming a stable nanotracer suspensions based on prepared nanoparticles in aqueous solutions of surfactants such as ammonium oleate and dimethylamine salt of oleic acid has been demonstrated. The particle size of the nanotracer has been determined by the Nanoparticle Tracking Analysis (NTA) method based on direct visualization and analysis of nanoparticles in aqueous media containing two types of surfactants. It has feen found that the medium size of nanoparticles doesn’t exceed 90 nm. The possibility of using the prepared

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