d10金属四硫代砷酸盐的合成与研究

Eearth Pub Date : 2015-07-23 DOI:10.11648/j.earth.s.2015040501.25

I. Didbaridze, M. Rusia, K. Rukhaia

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摘要

首次在水化学条件下合成了由Ag3AsS4和M3(AsS4)2•H2O组成的d10金属四硫代砷酸盐，其中M-Zn, Cd或Hg, X=(Zn)或2(Cd, Hg)。通过热分析、红外光谱、x射线晶体测定和衍生学研究，研究了其组成、组成、脱水反应和20-1000区间的抗热震性。

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Synthesis and Study of Tetrathioarsenates of d10-Metals

For the first time in hydrochemical conditions tetrathioarsenates of d10-metals by composition Ag3AsS4 and M3(AsS4)2•H2O, where M-Zn, Cd or Hg and X=(Zn) or 2(Cd, Hg), were synthesized. Their composition, constitution, reaction of dehydration and thermal shock resistance in 20-1000 interval were studied by means of thermal analysis, UR-spectroscopy, X-ray crystal determination and derivatographic research.

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Eearth

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