Kitosan的成分对蓖麻油的纳米纤维复合材料的影响

Ayuzia Puspa Indah, Alimin Mahyudin
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引用次数: 0

摘要

研究了壳聚糖组分对以蓖麻油为增塑剂的槟榔纳米纤维复合膜物理性能和生物降解性能的影响。采用溶液铸造法制备样品。壳聚糖用量为0 g、0.56 g、0.7 g、0.84 g、1.4 g,其中一个样品使用淀粉,壳聚糖用量为0.84 g。对试样的物理性能进行了厚度测试、FTIR测试和FESEM测试。机械性能测试包括抗拉强度、伸长率、弹性和生物降解测试。采用粒径分析仪(PSA)测定纳米纤维的粒径,场发射扫描电镜(FESEM)测定样品的形貌,傅里叶变换红外(FTIR)测定样品的官能团。PSA结果表明,纳米纤维的直径为(79 ~ 187)nm。FESEM表征结果获得了中空可生物降解塑料表面的形状。FTIR结果表明,降解塑料中存在C=O官能团,且C-O为亲水性官能团,表明生物降解塑料具有降解能力。在不添加淀粉的情况下,0.84 g壳聚糖的抗拉强度最佳,为20.04 MPa;在0.7 g壳聚糖的情况下,伸长率最佳,为138.56%;在0.84 g壳聚糖添加淀粉时,弹性最佳,为198.66 MPa,平均厚度为0.25 mm。壳聚糖含量变化越大,生物降解塑料的厚度、抗拉强度、弹性和生物降解率均增加,伸长率降低
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Pengaruh Komposisi Kitosan Terhadap Sifat Fisis Dan Biodegradable Film Komposit Nanoserat Pinang Dengan Castor Oil Sebagai Plasticizer
Research has been carried out on the effect of chitosan composition on the physical and biodegradable properties of areca nut nanofiber composite films with castor oil as a plasticizer. Samples were made using the solution casting method. The variations of chitosan used were 0 g, 0.56 g, 0.7 g, 0.84 g, 1.4 g and one sample used starch with a variation of 0.84 g chitosan. The physical properties of the samples tested were thickness test, FTIR test and FESEM test. Mechanical properties tests include tensile strength, elongation, elasticity, and biodegradation tests. The samples were characterized using a Particle Size Analyzer (PSA) to determine the size of the nanofibers, a Field Emission Scanning Electron Microscope (FESEM) to determine the sample morphology and Fourier Transform Infrared (FTIR) to determine the functional groups. PSA results showed that the nanofibers had a diameter of (79-187) nm. The results of FESEM characterization obtained the shape of a hollow biodegradable plastic surface. The FTIR results indicate the presence of a C=O functional group and C-O is a hydrophilic functional group which indicates that biodegradable plastic is capable of being degraded. The best tensile strength results in the chitosan variation of 0.84 g without starch with a value of 20.04 MPa, the best elongation in the 0.7 g chitosan variation with a value of 138.56%, elasticity 198.66 MPa in the 0.84 g chitosan variation with the addition of starch, the average thickness is 0.25 mm. The higher the variation of chitosan, the thickness, tensile strength, elasticity, and biodegradation of biodegradable plastics increase, while elongation decreases
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