Nilam C. Dige, Chandrama Randive, Omkar Tamhane, Rushikesh Ghorpade, S. Kale, Prasad G Mahajan
{"title":"基于morpholine的新型离子液体用于三唑烷硫酮的合成、表征及其生物学性质","authors":"Nilam C. Dige, Chandrama Randive, Omkar Tamhane, Rushikesh Ghorpade, S. Kale, Prasad G Mahajan","doi":"10.21926/cr.2301011","DOIUrl":null,"url":null,"abstract":"Keeping the green chemistry approach in mind we have synthesized a novel morpholine-based ionic liquid [NBMMorph]<sup>+</sup>Br<sup>-</sup>. The structure of Ionic liquid was confirmed by spectral techniques <em>viz</em>. IR, <sup>1</sup>H NMR, and<sup> 13</sup>C NMR, analysis. The synthesized novel IL [NBMMorph]<sup>+</sup>Br<sup>-</sup> was utilized to prepare 1,2,4-triazolidine-3-thiones of biological significance. The [NBMMorph]<sup>+</sup>Br<sup>- </sup>IL shows excellent catalytic activity, and a simple filtration technique can separate the thiazolidinedione products. The structure of the synthesized compounds were confirmed using IR and NMR techniques. All the synthesized compounds were screened for their antimicrobial activity. All compounds shows outstanding biological activity.","PeriodicalId":178524,"journal":{"name":"Catalysis Research","volume":"13 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Morpholine-Based Novel Ionic Liquid for Synthesis and Characterization of Triazolidinethiones and Their Biological Properties\",\"authors\":\"Nilam C. Dige, Chandrama Randive, Omkar Tamhane, Rushikesh Ghorpade, S. Kale, Prasad G Mahajan\",\"doi\":\"10.21926/cr.2301011\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Keeping the green chemistry approach in mind we have synthesized a novel morpholine-based ionic liquid [NBMMorph]<sup>+</sup>Br<sup>-</sup>. The structure of Ionic liquid was confirmed by spectral techniques <em>viz</em>. IR, <sup>1</sup>H NMR, and<sup> 13</sup>C NMR, analysis. The synthesized novel IL [NBMMorph]<sup>+</sup>Br<sup>-</sup> was utilized to prepare 1,2,4-triazolidine-3-thiones of biological significance. The [NBMMorph]<sup>+</sup>Br<sup>- </sup>IL shows excellent catalytic activity, and a simple filtration technique can separate the thiazolidinedione products. The structure of the synthesized compounds were confirmed using IR and NMR techniques. All the synthesized compounds were screened for their antimicrobial activity. All compounds shows outstanding biological activity.\",\"PeriodicalId\":178524,\"journal\":{\"name\":\"Catalysis Research\",\"volume\":\"13 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-03-12\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Catalysis Research\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.21926/cr.2301011\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Catalysis Research","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.21926/cr.2301011","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Morpholine-Based Novel Ionic Liquid for Synthesis and Characterization of Triazolidinethiones and Their Biological Properties
Keeping the green chemistry approach in mind we have synthesized a novel morpholine-based ionic liquid [NBMMorph]+Br-. The structure of Ionic liquid was confirmed by spectral techniques viz. IR, 1H NMR, and 13C NMR, analysis. The synthesized novel IL [NBMMorph]+Br- was utilized to prepare 1,2,4-triazolidine-3-thiones of biological significance. The [NBMMorph]+Br- IL shows excellent catalytic activity, and a simple filtration technique can separate the thiazolidinedione products. The structure of the synthesized compounds were confirmed using IR and NMR techniques. All the synthesized compounds were screened for their antimicrobial activity. All compounds shows outstanding biological activity.
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