层状压缩Zr-4合金不同变形区的组织、织构及力学性能

Jie Ren, Geping Li, Fusen Yuan, Ben Wang, Fuzhou Han, Muhammad Ali, Yingdong Zhang, Wenbin Guo, Bo Gao
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引用次数: 0

摘要

本文对具有片层组织的压缩Zr-4合金的非均匀塑性变形进行了系统的研究。在650℃的压缩试验中,还原率为70%的Zr-4合金形成了严重变形区(SDA)和困难变形区(DDA)。利用电子后向散射衍射(EBSD)和维氏硬度计研究了DDA和SDA的显微组织、织构和力学性能的差异。结果表明:由于动态再结晶(DRX)的发生,SDA中出现了大量等轴晶,而粗片层晶仍是DDA的主要组织,说明DDA是初始合金与SDA的中间产物。进一步提出了不连续再结晶机理。根据电子背散射衍射(EBSD)分析,SDA和DDA形成的优势织构使其α相{0001}面的法线方向平行于压缩方向,SDA形成的另一个更强的织构使部分{0001}面的法线方向偏离压缩方向~ 15°。SDA和DDA的织构差异主要是由DRXed晶粒造成的。为了评价SDA对Zr-4合金力学性能的影响,采用显微硬度试验。与DDA相比,SDA中的合金得到了强化,这是由于晶粒的细化和织构的多样化。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Microstructure, Texture and Mechanical Properties in Different Deformation Regions of the Compressed Zr-4 Alloy With Lamellar Structure
In the present work, the inhomogeneous plastic deformation of the compressed Zr-4 alloy with lamellar structure has been studied systematically. In the compression test of Zr-4 alloy with reduction of 70% at 650°C, the severe deformed area (SDA) and difficult deformed area (DDA) formed. The differences in DDA and SDA including microstructure, texture, and mechanical properties were investigated, using electron backscattering diffraction (EBSD) and Vickers hardness tester. The results showed that a large number of equiaxed grains appeared in SDA due to the occurrence of dynamic recrystallization (DRX), while coarse lamellar grains were still the main microstructure in DDA, showing that the DDA was the intermediate between the initial alloy and SDA. Furthermore, the discontinuous recrystallization mechanism was proposed. According to electron backscattered diffraction (EBSD) analysis, the predominant texture formed in SDA and DDA made normal direction of its {0001} planes of α phase parallel to the compression direction, and another stronger texture in SDA made the normal direction of part {0001} planes ∼15° away from the compression direction. The observed texture difference in SDA and DDA mainly resulted from the DRXed grains. To evaluate the influence of SDA on the mechanical properties of the Zr-4 alloy, microhardness tests were employed. The alloy in SDA had been proved to be strengthened compared to DDA, which was due to both the grain refinement and the texture diversity.
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